GCMS analysis results for sample AE12673, June 2002

NYC 9/11 Public Portal Document

Library Search Compound Report Data File C:\HPCHEM\l\DATA\MAY3102\12673.D Vial: 18 Acq On 1 Jun 2002 4:43 am Operator: Morgan Sample gc/ms scan 5/30 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0531.M (RTE Integrator) .. Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 Butanoic acid, methyl ester Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T. 5.22 0.66 ug/1 47271 1,4-Dichlorobenzene-d4 12.06 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Butanoic? acid, methyl ester 102 C5H10O2 000623-42-7 78 2 3-Buten-2-ol, 2-methyl- 86 C5H10O 000115-18-4 25 3 Butanoic acid, 2-propenyl ester 128 C7H1202 002051-78-7 17 4 3-Pyrrolidinol 87 C4H9NO 040499-83-0 9 Abundance Scan 19 (5.216 min): 12673.D (-) m/z 42.95 100.00% 43 74 A_

5000 59 87 37, 51 I 5.10 5.20 5.30 5.40 5.50 5.60 ■ ■ i ■ ■ • ■ i ■ ■ ■ ■ i ■ — 000,0000011 J____ ’ • l ' m/z 73.95 100.00% miz-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #63491: Butanoic acid, methyl ester 43 74

5000 TPPPAPmTTT 5.10 5.20 5.30 5.40 5.50 5.60 59 87 15 27 m/z 70.95 75.91% I 33 ■ ' i ■ 1 ■ ■ i ■ • ■ ■ i ■ ■ ■ ' i 1 ' 1 1 1 1 1 1 ' I 1 1 ' 1 r1 102 ■ ■ i ■ ■ ■ ' I ■ ■ ■ • i ' • ■ ■ i m/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #62855:3-Buten-2-ol, 2-methyl- 71 43 1tr 5.10 5.20 5.30 5.40 5.50 5.60 5000 m/z 58.90 34.01% 59

+ 27 53 86 1 1 । ■ ' ■ i ■ • ■ ■ I' ■ 1 1 i ■ -1 • ' ' i ■ ■ 1 ■ i ■ ' ■ ■ i ■ ■ ■ ' i mfz—> 10 20 30 40 50 60 70। 80 90 100 110 Abundance #4955: Butanoic acid, 2-propenyl ester 43 71 mA ■ i ‘ । • 11 * i * 11 ■ j 5.10 5.20 5.30 5.40 5.50 5.60 m/z 40.95 30.06% 5000 27 57 1 38 । • 11 11 ‘ ‘ ■ i ' • ‘ 89 100 ■ i * ■ ■ 1 I 1 1 1 1 I mmmAMM m/z—> 10 20 30 40 50 60 70 80 90 100 110 5.10 5.20 5.30 5.40 5.50 5.60

12673.D GCMS0531.M Mon Jun 03 11:44:54 2002 Page 1

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