GCMS sample AE05064 analysis, April 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\MAR3OO2\5151.D Vial: 37 Acq On : 31 Mar 2002 4:40 am Operator: Sample : gc/ms scan 3/8 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 2-Butanol, 3,3'-oxybis- Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T.

11.88 0.34 ug/1 41407 1,4-Dichlorobenzene-d4 12.25

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Butanol ,3'-oxybis- 054305-61-2 64 162 C8H18O3 2 1-Propano 2-(2-hydroxypropoxy) - 134 C6H14O3 000106-62-7 59 3 2-Propano' 1-(2-methoxy-1-methylet 148 C7H16O3 020324-32-7 56 _4 2-Propan6 1,1'-[(1-methyl-l,2-eth 192 C9H20O4 001638-16-0 40 Abundance'..... ( .. Sea ... m/z’... -597^..... 10 q";oo% 5)9

5000 45 73 103 ___ 11.60 11.80 12.00 12.20____ ■ 1^1'I" 11' 86 m/z 45.05. 46.93’% m/z->_____20 30 40 50 60 70 80 90 100 110 120 130 140 •Abundance” ............. ... ■ #1'28597^Butanol, S^S^oxybis-

.K 5(9

5000 31 45 L 103 11.60 11.80 12.00 12.20 m/z 103.05, 32.18% , I ............................ 1^ ' I ' ' ' ' I ' 'mZz-> 20 30 40 50 60 70_ 80 90 100 110 120 130 140 Abundance ^6086: 1-Prepanol. 2-i2'hvdraxyp-opoxv)- ! 59

11'60 11'80 12t0 12.20 5000 m/z 73.00, 28.78% 31 45 103

.... 75... 89....................... m/z-> 20 30 40 __ 50___60.__ 70__ 80___ 90__ 100__ 110__ 120__ 130 140 Abundance #9238'. 2-Propanol, 1-(2-niethoxy-1-methyiethoxy)- 5|9 11.60 11.80 12.00 12.20 I m/z 41.05 22.83% 5000 45 103 73 31

; . ............................. [ , ................130.......... H ' I ' I ' ■ I . . , . I . m/2-> 20 30 40 50 60 70 80 90 100 110 120 130 140 11.60 11.80 12.00 12.20

5151.D GCMS0308.M Tue Apr 02 15:38:31 2002 Page 2

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