GCMS sample analysis report for AD29791, Jan 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\DEC1401\29789A.D Vial: 51 Acq On : 16 Dec 2001 3:30 pm Operator: 209 GALOS Sample : gems scan 12/11 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 2-Butanol, 3,3'-oxybis- Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

11.44 0.42 ug/1 103074 1,4-Dichlorobenzene-d4 11.67

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Butanol, 3,3'-oxybis- 162 C8H18O3 054305-61-2 59 2 2 - Propanol , 1-(2-methoxy-1-methylet 148 C7H16O3 020324-32-7 56 3 1-Propanol, 2-(2-hydroxypropoxy)- 134 C6H1403 000106-62-7 53 4 2-Propanol, 1,1‘-[(1-methyl-1,2-eth 192 C9H20O4 001638-16-0 40 Abundance

m/z-> 5000

Abundance 20 Lll + — 60 + 70 80 30 45

51 84...... ।............... 90 100 110 120 130 140 40 50 Scan 697 (11.439 min): 29789A.D (-) 59

m/z 44.95 73

#12859: 2-Butanol, 3,3'-oxybis- 103 m/z

NJ 59.05 100.00%

11.20 11.40 11.60 11.80 48.84%

59

5000 31 45 103 11.20 11.40 11.60 11.80 m/ z 103.05 34.53%

m/z-> 20 -------- 30 40 + 50 ■ ■ । I60 ra ' 70 80 ......................................................... 134 , 90 100 110 120 130 140 Abundance i#9238: 2-Propanol, 1-(2-methoxy-1-methylethoxy)- 59 —M-—T 11.20 11.40 11.60 11.80 5000 45 103 m/z 41.05 27.46%

NN 73 I 31 l . i ....... 130.... ' i ■ 1 ' ' i ' 1 ■ ' i ' ■ i ' 1 ' ■ I ■ ' 1 1 i 1 ' ' ' i ■ ■ ' ' i ' ' ' ' i ' m/z-> 20 30 40 50 60 70 80 90110 120 130 140 100 Abundance #6086: 1-Propanol, 2-(2-hydroxypropoxy)- ------------ 59 11.20 11.40 11.60 11.80 m/Z 73.00 6.34% . 5000

miz- 31

-P+ther TTrrpeTuumuu 20 75 30 89 —TT 40 45

50 (60 70 80 90 100 103

113 120 130 140 -M. 29789A.D GCMS1126.M Wed Jan 30 11:48:37 2002 Page 2

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