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GCMS analysis results for sample AD29925, Jan 2002

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Laboratory report of GCMS analysis for sample AD29925 conducted on January 7, 2002.

NYC-WTC_000036972–000036982

Folder label: “GCMS X 12/10/01 A 12/15/01

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NYC 9/11 Public Portal Document ,Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC1401\29925.D Vial: 13 Acq On : 15 Dec 2001 2:15 pm Operator: 209 GALOS Sample : gems scan 12/10 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 2-Butanol, 3,3'-oxybis- Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

11.43 1.39 ug/1 341914 1,4-Dichlorobenzene-d4 11.68

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Butanol, 3 ,31 -oxybis- 162 C8H18O3 054305-61-2 64 2 2-Propanol, -(2-methoxy-1-methylet 148 C7H16O3 020324-32-7 56 3 2-Propanol/ 1-(2-methoxypropoxy)- 148 C7H1603 013429-07-7 40 4 2-Propanol, 1,1'-oxybis- 134 C6H14O3 _______ 000110-98-5 39 Abundance Scan 695 (11.428 min): 29925.D (-) m/z 59.05 100.00% 59

5000

39 ■ i ■ —4+ .... r — - -III 45 73

85 103 M I ' ' ' ' I ' ' ' ' I 11.00 11.20 11.40 11.60 11.80 m/ z 44.95 48.64% m/z-> 20 30 40 !50 60 70 80 90 100 110 120 130 140 Abundance #12859: 2-Butanol, 3,3'-oxybis- 59

5000 - 31 ■ ' 1 ■ । ■ ■ ' 1 । ■ • ■ ' । ' 1 ■ 45 103 11.00 11.20 11.40 11.60 11.80 m/z 103.05 34.11% ---------- # . . ....................................................134. m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance ;#9238: 2-Propanol, 1-(2-methoxy-1-methylethoxy)- 59 T—TT— 11.00 11.20 11.40 11.60 11.80 m/z 73.00 2 8.11%

NA 5000 - 103 45 73 । 31 I I . ‘IT1 ..............1..... 130... • i ■ ■ ■ ' i ■ miz--> 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #9233: 2-Propanol, 1 -(2-methoxypropoxy)- 59 11.00 11.20 11.40 11.60 11.80 m/ z 41.05 24.01%

m/z—> 5000-

........... I • f > ■ ■ ■ f > 20 31

30 40 45

50 —60. 701..... 80 194 .. -120— TTMPITTT 90 100 110 120 130 140 11.00 11.20 11.40 11.60 11.80 . NN 29925.D GCMS1126.M Fri Dec 28 13:28:11 2001 Page 3

NYC-WTC_000036981

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