GCMS sample analysis report for AD29791, Jan 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\1\DATA\DEC14 01\29789A.D Vial: 51 Acq On 16 Dec 2001 3:30 pm Operator: 209 GALOS Sample : gems scan 12/11 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 Silane, tetramethyl- Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

7.59 4.45 ug/1 1091130 1,4-Dichlorobenzene-d4 11.67

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Silane, tetramet 88 C4H12Si 000075-76-3 9 2 N-Ethyl formamide 73 C3H7NO 000627-45-2 9 3 Pentane, 3-methoxy- 102 C6H140 036839-67-5 9 4 1,3-Diox olane, 2-(3-bromo-5,5,5-tri 352 C10H16BrC13O2 000000-00-0 9 Abundance Z Scan 278 (7.593 min): 29789A.D (-) m/ z 73.00 100.00% 73

5000 43 TIPIIPIITTTTT 87 103 7.20 7.40 7.60 7.80 8.00 -_____ ____ , | 50 55 60 67, । 1——T l ■ ■ i ■ • •' t i > > • ■ i ‘ > i ■ m/ z 43 .on 29.13% miz-> 10 20 30 40 50 60 70 80 90 . 100 110 Abundance #62932: Silane, tetramethyl- 73

I 1 । । — 5000 7.20 740 7.60 7.80 8.00 45 m/ Z 41.05 10.50% 15 - - I 53 59 |............. 88............................... m/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #292; N-Ethylformamide 30 73 -TIITT 7.20 7.40 7.60 7.80 8.00 . 5000 m/Z 4 5.05 10.41% 44 58

15 .1 I m/z-> 10 20 30 40 50 60____ 70____ 80 90 100 110 Abundance #1793: Pentane, 3-methoxy- 1 rrr It— -11187 I -r-r 73 7.20 7.40 7.60 7.80 8.00 m/ z 71.00 6.72% 5000 45

733 39 . • * i > > ■ ■ i ■ ■ ' • i ■ ■ ■ 'i । ■ ■ 55 TT i- । (-n-r-|-T —I—mm InBB—nm—B—T—TT TTRT । 10 20 30 40 50 60 70 80 90 100 110 7.20 7.40 7.60 7.80 8.00

29789A.D GCMS1126.M Wed Jan 30 11:48:33 2002 Page 1

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