GCMS analysis results for sample AD30490, Jan 2002

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Data File : C:\HPCHEM\1\DATA\DEC3101\30490.D Vial: 12 Acq On : 31 Dec 2001 9:40 pm Operator: 209 GALOS Sample : gems scan 12/14fb Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 Silane, tetramethyl- Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

7.61 4.15 ug/1 1122500 1,4-Dichlorobenzene-d4 11.68

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Silane, tetramethyl- 88 C4H12Si 000075-76-3 9 2 Butane, 2-methoxy-2-methyl- 102 C6H140 000994-05-8 9 3 3-Pentanol, 3-methyl- 102 C6H140 000077-74-7 9 4 N-Ethylformamide 73 C3H7NO 000627-45-2 5 Abundance 7 scan 280 (7.612 min): 30490.D (-) m/z 73.0.0 100.00% ' 73

। 5000 43 I ' ' ' ' I ' ' 1 ‘ I ‘ ‘ 1 1 1 I ‘ • 87 103 7.20 7.40 7.60 7.80 8.00 | 50 55 50 67, t , 1’4 I | t ‘ I f‘t { T I' J ‘ I | t 11—0—9——————— m/z 43.0,5 31.46% m/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #845: Silane, tetramethyl- 73 %

5000 i ■ ■ ■ ■ i ' • • ■ i ‘ ■ i • 1 ■ i • ■ 7.20 7.40 7.60 7.80 8.00 45 m/z 45.0,5 11.86% 15 *1**TT-I*114 100008 31 . J 55 1 88 > | > I I I J ! I t I J I J I I J 1 miz-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #1761; Butane, 2-methoxy-2-methyl- 73 i1 1 • 1 i ' 1 • ' i 1 1 ' IId" —it T‘ ■ 7.20 7.40 7.60 7.80 8.00 5000 m/ z 41.0,5 11.82% 55 87 45 27 33 i i, miz-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #63572: 3-Pentanol, 3-methyl- —TTTgTTerm . 73 7.20 7.40 7.60 7.80 8.00 m/z 71.00 6.80% 5000 55 45 87 27 | ! CC re .. i ‘ 1 ■ ‘ i ‘ • 1 ‘ i ‘ 1 ' ' 113 PTl’t 1 miz-> 10 20 30 40 50 60 70 80 90 100 110 7.20 7.40 7.60 7.80 8.00

30490.D GCMS1126.M Wed Jan 16 08:28:09 2002 Page 1

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