GCMS sample AE05064 analysis, April 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\M7VR3002\5151.D Vial: 37 Acq On : 31 Mar 2002 4:40 am Operator: Sample : gc/ms scan 3/8 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L if********************************************************************

Peak Number 1 N-Ethylformamide Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

8.13 0.76 ug/1 93.885 1,4-Dichlorobenzene-d4 12.25

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 N-Ethylf(^mamide 73 C3H7NO 000627-45-2 9 2 2-Butanc^e, 3-methoxy-3-methyl- 116 C6H12O2 036687-98-6 9 3 1,3-Dio3tolane, 2-(3-bromo-5,5,5-tri 352 C10H16BrC13O2 000000-00-0 9 4_3-Pent^nol, 3-methy]^ _ ______ 102 C6H14O 000077-74-7 9 Abundance ..... .......... Scan 336'(8?i’33'rT)in): 5151.D"(-) m/ z 73.0,0 Tb ioo'.’oo%

5000 43

103 7.80 8.00 8.20 8.40 ’m/z~> 10 ' I ' ' ' ' I ' ' ' ' I ' ' ■ ' I ' ■ ' ' I ' ' ' ' ( ' m/ z 43.05 28.55% 20 30 40 50 60 70 80 90 100 110 120 Abundance ■ #292; N-Ethylformamide Sb 73

5000 ' ' I ’ ' ' ' 1 ' ' ' ' I ' 44 5S 7.80 8.00 8.20 8.40 m/ z 40.95 11.63% 15 I ' I ' ' ' ' I ' ' ' ' I ’ ' ' ' I ' ' ' ' 1 ' ' ' ' I ‘ ‘ I ' 'm/z-> 10 20 40 50 60 70 80 90 100 110 120 Abundance #3263. 2-Biitenone 3-methoxy-3-met}iyl- 73 —i-A 43 7.80 8.00 8.20 _8^_____ 5000 m/ z 9.58%

57 85 101 ' I ' ' ' I ’ ' ' ' I ' ' ' ' i ' ' I ’ • » ' I '■» » » j I m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 Abundance #49423; 1.3-Dioxolane, 2-(3-bromo-5,5,5-lrichloro-2,2-dimef 7{3 8^0 7.80 8.20 8.40 m/z 7.17%' 5000 45 6,6 I I 55 67, r-r-r-r-r-rrn-r-r-r-T-r-r^^

'm/z-> 10 20 30 40 50 60 70 80 90 100 110 120 7.80 8.00 8.20 8.40

5151.D GCMS0308.M Tue Apr 02 15:38:27 2002 Page 1

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