GCMS analysis report, sample AE04450, April 2002

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\MAR2102\4450.D Vial: 13 Acq On : 21 Mar 2002 11:07 pm Operator: Sample : gc/ms scan 3/1 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 N-Ethylformamide Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 8.14 2.22 ug/1 362197 1,4-Dichlorobenzene-d4 12.26 Hit# of 5 entative ID MW MolForm CAS# Qual 1 N-Ethylfo: amide 73 C3H7NO 000627-45-2 9 2 Silane, t ramethyl- 88 C4H12Si 000075-76-3 9 3 1,3-Dioxo ane, 2-(3-bromo-5,5,5-tri 352 C10H16BrC13O2 000000-00-0 9 4 1-Butanamline, 3-methyl- 87 C5H13N 000107-85-7 7 Abundance - Scan 337 (8.143 min): 4450.D (-) m/z 73.00 100.00% 73

5000 43 7.80 8.00 8.20 8.40 , I, | 50 55 TIpm 67, i , 87 mmmpor 103 i j r 1T—— m/z 43.05 29.21% m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 Abundance #292: N-Ethylformamide 30 73

5000 —uummTmTTTTT 58 7.80 8.00 8.20 8.40 44 m/z 41.05 10.95% 15 — 1 i ■ ■ • ■ i ■ 1 ■ ■ i • ‘ ' i ■ ■ ■ ■ i ‘ ■ i • ■ ■ ■ i ■ ■ mfz~> 10 20 30 40 50 60 70 80 90 100 110 120 Abundance #62932; Silane, tetramethi- 73 TdRmmmOfTTTTT 7.80 8.00 8.20 8.40 5000 m/z 45.05 10.42% 45 15 , , 53 59 88 ■ • i ■ • ■ ■ i ■ ■ • ■ i ■ ■ '"r l ‘ 1 I"f i r i i i | i rj tj 1 i miz-> 10 20 30 40 50 60 70 80 90 100 110 120 Abundance #49423: 1,3-Dioxolane, 2-(3-bromo-5,5,5-trichloro-2,2-dimet —PIIIPTPm tB 73 7.80 8.00 8.20 8.40 m/z 71.00 7.03% 5000 45 ................ 3611| t» 55 j » * * * । i > i i । i i i i । i ! r ■ i 1 ‘ 1 ■ i ■ • ■ ■ i 1 67 H ■ i ■ • 1 1 i • ■ ‘ 1 i ■ ■ ■ 109115 ■ i 1 ■ ■ ■ i ■ ■ m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 7.80 8.00 8.20 8.40 “ '

4450.D GCMS0308.M Fri Mar 22 09:44:16 2002 Page 1

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