GCMS analysis report, sample AE04451, April 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\MAR2102\4451.D Vial: 14 Acq On : 22 Mar 2002 12:06 am Operator: Sample : gc/ms scan 3/1 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 N-Ethylformamide Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

8.15 2.26 ug/1 402981 1,4-Dichlorobenzene-d4 12.27

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 N-Ethylformamide 73 C3H7NO 000627-45-2 9 2 Silane, tetramethyl- 88 C4H12Si 000075-76-3 9 3 1-Butanamine, 3-methyl- 87 C5H13N 000107-85-7 7 4 1 - Pent anami ne 87 C5H13N _______ 000110-58-7 4 Abundance Scan 338 (8.146 mln): 4451 .D (-) . m/z 73.00 1 00.00% 73

5000 43 ■ ■ i ■ ■ ‘ ■ i 1 ■' • i 18, i • > ■ • i ‘

T 7.80 8.00 8.20 8.40 miz-> ................................. • ■ i ■ ' • ■ i ■ ■ ■ ■ i ■ ■ ■ 1 I1 10 20 30 .... + 40 50 55 TIEdnnnIr 50 60 67,1 ,l-ri grTri 70 80 87 103 j i i ■ ■ । i' ■ i i । r 90 100 110 m/z 43.05 27.84% Abundance #292: N-Ethylformamide 30 73

5000 7.80 8.00 8.20 8.40 1 44 58 m/z " 9.88% 15 : 1 1 1 1 1 1 ' 1 ।1 1 — ■ i • ■ i ■ ■ ■ ' i ' 1 ■ ‘ i • ' • ‘ i ■ ' • • i ‘ ' ■ i ‘ miz-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #845 < Selane, ttrarnethyl- 73

7.80 8.00 8.20 8.40 5000 m/z 41.05 9.60% 45 15 31 i i 55 88 m/z-> 10 2030405060 70 8090 100 110 Abundance #763: 1-Butanamine, 3-methyl- 33 7.80 8.00 8.20 8.40 m/z 71.0.0 6.39% 5000

15 41 70 87 m/z-> ■ ■ i ‘ 10 ' i ‘ ' 20 '30r- ri I’ 40 I 50 55 60 70 80 90 100 110 ...................... . ■ ■ i ■ ■ ‘ 1 i ■ ' 1 ■ i • ■ 1 ■ i ■ 1 ‘ ‘ i ‘ 7.80 8.00 8.20 8.40

4451.D GCMS0308.M Fri Mar 22 09:45:00 2002 Page 1

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