GCMS analysis results, sample AE04946, April 2002

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Library Search Compound Report

Data File C: \HPCHEM\l\DATA\M7kR3002\4946 .D Vial: 13 Acq On 30 Mar 2002 2:52 am Operator: Sample gc/ms scan 3/6 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 N-Ethylformamide ' Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

8.14 0.30 ug/1 33658 1,4-Dichlorobenzene-d4 12.25

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 N-Ethylformamide 73 C3H7NO 000627-45-2 9 2 Butane, 2-methoxy-2-methyl- 102 C6H14O 000994-05-8 9 3 Pentane,/3-methoxy- 102 C6H14O 036839-67-5 9 4 Formamic^, N, N-dimethyl- 73 C3H7NO ______ 000068-12-2 5 Abundance 1 Scan 337 (8.140 rnin): 4946.DT-) m/z ”73.00 ”10 0.00% 7)3

5000 43

39 ■49, I 55 59 69, 7.80 8.00 8.20 8.40 84 87 . ......... ........................... " I' I" I " " I' m/z 43.05’ 29.60% m/Z“>..... _5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance' #292: N-Ethylformamide 3l0 73

5000 . „ ./V 44 58 7.80 8.00 8.20 8.40 27 m/z 44.95 10.05% 15 ! . ..... m/z-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #1761, Butane. 2-(netboxy-2-mettivl- 73 . .............\ , ’ P ' ' ' I 7.80 8.00 8.20 8.40 5000 m/z 41.05 8.76% 55 87 2.7 33 45 i 59 70 1 I' ‘' I' m/z-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #1793: Pentane, 3-meth6xy- ‘ I ‘ ' I 7|3 7.80 8.00 8.20 ^40___ _ m/z 7.95% 5000 41 45

,TTTTTTT,.nXrTArrT+T^^ 70 +t 'm/z-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 "go '95 J 7.80 8.00 8.20 8.40

4946.D GCMS0308.M Tue Apr 02 11:08:56 2002 Page 1

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