GCMS analysis results, sample AE04946, April 2002

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Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\MAR3002\4946.D Vial: 13 Acq On : 30 Mar 2002 2:52 am Operator: Sample : gc/ms scan 3/6 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M. (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ***’******************************************************************

Peak Number 2 Cyclopentasiloxane, decamethyl Concentration Rank 1

R.T. EstConc Area Relative' to ISTD R.T.

14.85 1.36 ug/1 197304 Naphthalene-d8 15.89

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Cyclopentaslloxane, decamethyl- 370 C10H3005Si5 000541-02-6 53 2 3,4-Dihydrc^ymandelic acid, ethyl e 428 C19H36O5Si3 000000-00-0 47 3 Phenethylarfiine, N-methyl-.beta.,3,4 399 C18H37NO3Si3 010538-85-9 38 4 N-(Trifluotacetyl)-0,0',O"-tris(tri 495 C20H36F3NO4Si3 000000-00-0 38 Abundance Scan 1068 (14.851 min): 4946.D (-) 7(3 ft 267 355 5000

45 108 133 IM , 193 223 ‘249 j 323 14.60 14.80 15.00 15.20 tW m/z 267.00 52.50% m/z->____40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 400 Abundance #51266: Cyclopentasiloxane, decamethyl- 713

355 5000 267 I ( I ' ' ____ 14.60 14.80 15.00 15.20 m/z.355.05 52.01% 207 249 323 m/z->____ 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 400___ Abundance #55759. i4-t)!hv<lro;’ynriant!elic aad. ethyl ester. !ri-TMS 355 I I ' ' 73 14.60 14.80 15.00 15.20 5000 m/z 356.05 18.44%

208 251 281 385 413 m/z->____40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 400 Abundance #53791: Phenethylamine, N-meihyl.beta.,3,4-tris(trimethyls ' .............. 3; 5 i 14.60 14.80 15.00 15.20 m/z 268.00 13.33% 5000 73

51 130147 179 267 294 384 I ' ' m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 400 14.60 14.80 15.00 15.20

4946.D GCMS0308.M Tue Apr 02 11:09:01 2002 Page 2

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