GCMS sample analysis summary, April 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\MAR3OO2\485O.D Vial: 7 Acq On : 29 Mar 2002 8:54 pm Operator: Sample : gc/ms scan 3/6 fb Inst : GC/MS 209 • Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 N-Ethylformamide Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

8.15 0.31 ug/1 44220 1,4-Dichlorobenzene-d4 12.25

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 N-Ethylformamide 73 C3H7NO 000627-45-2 9 2 Formamide, N,N-dimethyl- 73 C3H7NO 000068-12-2 9 3 Butane, 2-mefc'hoxy-2-methyl- 102 C6H14O 000994-05-8 9 4 3-Pentanol,/3-methyl- 102 C6H14O 000077-74-7 9 Abundance Scan 338 (8.146 min): 4850.D (-) m/z. 737^..iooT^ 7)3

5000 43

3§ |,[.|... ,57, , I,I, I, ' ' I ' ' 87 103 7.80 8.00 L 8.20 8.40 ■33.0^ ■p

''' I ' ' ' ' I ''' ' ' I ' m/z 43.05 m/z-> 10 20 30 10. __ 50__ _60 70_ 80 90 100 110 Abundance #292: N-EthyifoFrnamide 30 73

5000 44 58 _ 7.80 8.00 8.20 8.40 m/z 41.0,5 12.18% ............ I , . . , I ''........ I ......... I . m/z->10 20 30 .40____ 50____ 60___ 70____ 80____ JO____ 100___ 110 Abundance #52527. Forinamido, N.N-d r.-elhyl- 44 73 p 7.80 8.00 8.20 8.40 5000 m/z 45.C5 8.26% 30 15 39 58 I ' ' ‘ ' I ' I ' ' ' ' I ' ' ' ' I m/z-->____ 10 20 30 40 50 60 70 80 90 100 110 Abundance #1761: Butane, 2-methoxy-2-methyl- 70 7.80 8.00 8.20 8.40 m/z 7.93% 5000 55 87 1 27 33 45 I I m/z-> 10 20 30 40 50 60 70 80 90 100 110 7.80 8.00 8.20 . 8.40

4850.D GCMS0308.M Tue Apr 02 11:04:36 2002 Page 1

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