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GCMS analysis results, sample AE05236, April 2002

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Laboratory report documenting GCMS analysis of sample AE05236 for unknown compounds on April 9, 2002.

NYC-WTC_000059185–000059195

Folder label: “GCMS X 3/9/02 A 3/30/02

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Scanned page image, NYC-WTC_000059192
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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\MAR3002\5236.D Vial: 47 Acq On : 31 Mar 2002 2:36 pm Operator: Sample : gc/ms scan 3/9 Inst :■ GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params:, LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 1 N-Ethylformamide Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

8.14 0.51 ug/1 63945 1,4-Dichlorobenzene-d4 12.25

Hit# of 5 tentative ID MW MolForm CAS# Qual

1 N-Ethylformamide 73 C3H7NO 000627-45-2 9 2 Pentane, 3-ymethoxy- 102 C6H14O 036839-67-5 9 3 1-Butanamine, 3-methyl- 87 C5H13N 000107-85-7 5 4 Octanal, 7/-methoxy-3,7-dimethyl- 186 C11H22O2 003613-30-74 Abundance i ...... ..........-....... "■siran 337 (8.136 min): 5236.D {-) 73 m/ z TJTojO... io oTo 0 % 1 5000 43

55 87 103 7.80 8.00 8.20 8.40 m/z 43.05 31.35% m/z-> 10 20 30 40 _50 60 __ 70 80 90 100 110 Abundance #292: N-Ethylformamide 30 I 73 I i I ' r'7.1 11 5000 58 __ 7.80 8.00 8.20 8.40 ! 44 I m/z 41.0,5 11.56% i

m/z-> I'o' ' ' '2'0 Ln 30 40 11.

50 60 70 80 90 100 110 Abundance #1793; Pentane, S-methoxy- 73 ‘<^1^ I 7.80 8.00 8.20 8.40 5000 m/z 45.00 9.71% ; 45

33 39 55 ' I ' ' ' I ' ' ' ' I ' ' ' ' I ' ‘ ‘ ' I ' ■ ' ' I ' ' ' ' I ' ' ' ' I ' rn/2--> 10 20 30 40 50 __ 60 70 ___ JO____ 90___100 110 Abundance #763: 1-Butanamine, 3-methyl- A 33 7.80 8.00__ 8.20 8.40 m/z 71.0.0 6.21% 5000

I ■I 15 41 55 70 87 A jn/z-> 10 20 30 40 50 60 70 80 90 100 110 7.80 8.00 8.20 8.40

5236.D GCMS0308.M Wed Apr 03 14:02:28 2002 Page 1

NYC-WTC_000059192

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NYC-WTC_000059192Source: NYC Law Department, mirrored locally

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