GCMS calibration analysis results, DEP Labs, Feb 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\FEB2102\1435.D Vial: 7 Acq On : 21 Feb 2002 8:00 pm Operator: Sample : gc/ms scan 1/22 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 1 N-Ethylformamide Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

8.21 0.36 ug/1 26848 1,4-Dichlorobenzene-d4 12.33

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 N-Ethylformamide 73 C3H7NO 000627-45-2 9 2 1,3-Dioxolane 74 C3H6O2 000646-06-0 7 3 l-Butanamine, 3-methyl- 87 C5H13N 000107-85-7 7 4 1 - But anami ne, 2-methyl- 87 C5H13N m/z 73 ... 100.00% 7 000096-15-1 Abundance 1 Scan 345 (8.207 min): 1435.D () 73

5000 43 7.80 8.00 8.20 8.40 8.60 i11 ■11"1 ■ i''1 ■ i' ■" i‘ i" .. . +84- m/z 42.95 30.28% m/z-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #292: N-Ethylformamide 30 73

5000 i ’ * i-r-r-|-r-r

44 7.80 8.00 8.20 8.40 8.60 27 m/ z 41.05 11.82% 15 — TRHT m/z->__ 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 ' i " • ■ i * ■" i" ■' i1 ■ ‘11 ■

Abundance 73 1*’’1’+**I’**I* 29 44 7.80 8.00 8.20 8.40 8.60 i 5000 m/z 44.95 10.53%! 15 19 26 wummummpunmumnmmummmmmmp m/z->__ 5. 10. 15 20 25 30 35 40 45 50. 55 60 65 70 75 80 85 90 95 Abundance #763: "i-Butanamine, 3-methyl- 30 7.80 8.00 8.20 8.40 8.60 m/z 71.00 7.41% 5000-

15 27 TTTTTTT ,4144 55 58 70 87 i ■ ■ ‘ ■ i 1 ■ ‘ ■ i ■ ■ i ■ ■ 1 1 i ■ • m/z-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 7.80 8.00 8.20 8.40 8.60

1435.D GCMS0208.M Fri Feb 22 09:30:55 2002 Page 1

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