GCMS analysis results for sample AD29733, Jan 2002

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Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC1401\29733.D Vial: 20 Acq On 15 Dec 2001 9:03 pm Operator: 209 GALOS Sample : gems scan 12/10 a Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title 209 625/TCLP calibration table Library C:\DATABASE\NBS75K.L

Peak Number 1 N-Ethylformamide Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

7.59 3.69 ug/1 989595 1,4-Dichlorobenzene-d4 11.67

Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 N-Ethyl forman ide 73 C3H7NO 000627-45-2 9 2 1-Butanamine, 3-methyl- 87 C5H13N 000107-85-7 7 3 1,3 -Dioxolane , 2-methyl- 88 C4H802 000497-26-7 5 4 Ethylamine___ 45 C2H7N 000075-04-7 4 Abundance Scan 278 (7.594 min): 29733.D (-) m/ z 73.00 100.00%! 73

5000 43 7.20 7.40 7.60 7.80 8.00 | 38.4 1 50 55 60 ' ■ i ' ' ' 1 1 1 ■ ■ ■ i ■ 67, । 1, . • i • • 87 103 ■'' i • 1 ■ ' i '' i ' ' m/z 43.05 28.95% m/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #292: N-Ethylformamide 30 73

5000 7.40 ' 7.60 7.80 8.00 58 7.20 44 m/ z 45.05 10.58% 15 1. .. i ■ ■ ■ ' i ■ 1 ■ ' i ■ • • ■ i ■ ■ 1 ■ i ■ ■ ■ ■ i ■

miz-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #763: 1-Butanamine, 3-methyl- 30

7.20 7.40 7.60 7.80 8.00 5000 - m/z 41.00 10.18%

15 41 55 70 87 i ' ■ ■ ' i m/z—> 10 20 30 40 50 60 70 80 90 100 110 Abundance #62902: 1,3-Dioxolane, 2-methyl- TadT . r । - Tm........ i । 73 7.20 7.40 7.60 7.80 3.00 rn/ z 71.00 6.39% 5000 43 58 27 87

m/z--> ! 7 ' ' T i' 10 20 30 40 +.. 50 ■ I ' ' ' ' I ' 1 ' ' I ‘ ■ I > ' ' ■ I ' TI—IT 1-1 7.20 7.40 7.60 7.80 8.00 60 70 80 90 100 110

29733.D GCMS1126.M Fri Dec 28 13:11:20 2001 Page 1

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