GCMS sample analysis results, Jan 2002

NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC1901\30021.D Vial: 7 Acq On : 19 Dec 2001 3:38 pm Operator: 209 GALOS Sample : gc/ms scan 12/12 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library- : C:\DATABASE\NBS75K.L

Peak Number 1 N-Ethylformamide Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

7.60 4.19 ug/1 944740 1,4-Dichlorobenzene-d4 11.67

Hit# of 5 entative ID MW MolForm CAS# Qual 1 N-Ethylformamide 73 C3H7NO 000627-45-2 9 2 1-Butanamine, 3-methyl- 87 C5H13N 000107-85-7 9 3 Silane, tetramethyl- 88 C4H12Si 000075-76-3 9 4 Pentane; 3-methoxy- 102 C6H140 036839-67-5 9 Abundance Scan 279 (7.603 min): 30021.D (-) m/z 72.9,5 100.00% 73

5000 43 1 I 74t I 1 1 87 7.20 7.40 7.60 7.60 8.00 38 I, I 48 55 67, f 103 ■ ' I ' ■ ‘ 1 I ' 1 1 1 I 1 1 ’ i'«'f‘ I' i i | ri'i'i'i i rri'i'i H • । ■ b • । ■ ■ ■ ■ । ‘-1 ■ ' । ■ m/ z 43.00 29.99% miz-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #292: N-Ethylformamide 30 73

5000 tt | r >

44 58 7.20 7.40 7.60 7.80 8.00 m/z 41.0,5 10.64% 15 —■ I... ■ l" ■ । ■ 1*1 rr 1 1 I ' । ' । I ' m/z-> 10 20 ;30 40 50 60 70 80 . 90 100 110 Abundance #763: 1-Butanamine, 3-methyl- 30 IIrni’m i1 ‘Tn ■ ■ । m i । r r 7.20 7.40 7.60 7.80 8.00 5000- m/z 44.95 10.64%

15 41 55 70 87 ' ■ i ■ ■ ■ ■ i ■ ■ ■ ■ i b ■ ■ • i ■ ■ ■ ■ i ‘ ■ i ■ ' ■ ■ i ■ ■ ‘ ' i ' ■ ‘ • i ‘ ' i 1 • ' ■ i ' m/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #845: Silane, tetramethyl- 73 T" 11 ITnm 1 ’* 7.20 7.40 7.60 7.80 8.00 m/z 71.0,0 6.84% 5000

15 31 , | 55 88 ■ ‘ I ‘ ‘ ‘ ‘ I • ‘ ' 'I1' । । ■ | H'r । । । I'Uf'i r i r i । i ■ ‘ i ■ ■ ■ 1 i ■ ■ ■ ' i ‘ ' i ‘ miz-> 10 20 30 40 50 60 70 80 90 100 110 7.20 7.40 7.60 7.80 8.00

30021.D GCMS1126.M Wed Jan 02 16:04:26 2002 Page 1

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