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GCMS analysis results for sample AD29926, Jan 2002

Machine-extracted title · confidence 100%

Gas chromatography-mass spectrometry report documenting analysis of sample AD29926 conducted on January 28, 2002.

NYC-WTC_000037352–000037362

Folder label: “GCMS X 12/11/01 A 12/18/01

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Scanned page image, NYC-WTC_000037359
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OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC1801\29932.D Vial: 16 Acq On : 19 Dec 2001 6:44 am Operator: 209 GALOS Sample : gc/ms scan 12/11 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 N-Ethylformamide Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

7.60 4.20 ug/1 1173830 1,4-Dichlorobenzene-d4 11.68

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 N-Ethylformami 73 C3H7NO 000627-45-2 9 2 Silane, tetramethyl - 88 C4H12Si 000075-76-3 9 3 Butane, 2-methoxy-2-methyl- 102 C6H140 000994-05-8 9 4 1-Butanamine, 3-methyl- 87 C5H13N 000107-85-7 7 Abundance /7 Scan 278 (7.599 min): 29932.D (-) m/ z 73.0,0 100.00% 73

5000 43 7.20 7.40 7.60 7.80 8.00

miz-> 0 | . n . pTiTf +4455.. . , 87 103 1 Tgg T’TT’IEETTT 1111 । .... । 10 20 30 40 50 60 70 80 90 100110120130140150160170180190200210 207 r "' i" " I m/ z 43.00 29.15% Abundance #292: N-Ethylformamide 30 73

5000 - 44 58 7.20 7.40 7.60 7.80 8.00 m/z 45.0,5 11.21% 15 Tp I’"" I "'i 111 "I""! | I t I I | I . I I |ll | . II . | . I M p > > > |

m/z-> 10 20 30 40 50 60 70 80 90 100110120130140150160170180190200210 Abundance #845: Silane, tetramethyl- 73 1 TIP—u/n1,, TuIndnTm 7.20 7.40 7.60 7.80 8.00 5000 - m/ z 41.05 10.80%

. 45 15 31 —,nutp TUOutOnp I —nunp 55 88 TUUTITTTTTTTT"T"T""TT‘TTT"TCTEI"ITTT‘TT m/z-> 10 20 30 40 50 60 70 80 90 100110120130140150160170180190200210 (Abundance #1761: Butane, 2-methoxy-2-methyl- TIIndT ——————— 73 7.20 7.40 7.60 7.80 8.00 m/ z 71.00 6.66% 5000 55 87 27 45 r"■i | Tr,”i TTITTTT ।1 ■ ■ ■ । * ■ ■ ■ ।* ।1 ■ ■ ■ ।। i•■■’। > I' • • ■ i11 ■ ■ I •1" I ■ •" l ” " i ■ m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 210 7.20 7.40 7.60 7.80 8.00

29932.D GCMS1126.M Tue Jan 15 15:26:08 2002 Page 1

NYC-WTC_000037359

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NYC-WTC_000037359Source: NYC Law Department, mirrored locally

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