GCMS analysis report for sample AE01227, Feb 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\FEB1802\1227.D Vial: 40 Acq On : 18 Feb 2002 4:05 pm Operator: 209 GALOS Sample : gc/ms scan 1/17 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 N-Ethylformamide Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

8.21 0.34 ug/1 25721 1,4-Dichlorobenzene-d4 12.33

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 N-Ethylformamide 73 C3H7NO 000627-45-2 9 2 Pent ane J 3-methoxy- 102 C6H140 036839-67-5 9 3 1-Butanamine, 3-methyl- 87 C5H13N 000107-85-7 7 4 Formamide, N,N-dimethyl- 73 C3H7NO 000068-12-25 Abundance Scan 345 (8.206 min): 1227.D (-) m/z 73.00. 100.00% 73

5000 43 ........ , I * * ‘ 4 I * ' ' 1 1 1 ‘ 51 55 59 69 7.808.00 8.20 8.40 8.60 m/z-> __ 5 39 1 Ttm 1....8487..... 10.. 15... 20 .. 25...30... 35 40 45 50 55 60 65 70 75.. 80 85 90 95 m/z 43.05 29.75% Abundance #292: N-Ethylformamide 30 73 _______ 5000 44 58 7.80 8.00 8.20 8.40 8.60 27 m/z 41.05 11.66% 15 41 miz—2 ' ■ “ i' mHH ' "|. ■■ 'll" ■ ■ i " • ■ i ■' 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 ■ i ■ ■ ■ ■ i ■ ■ ■ ■ i ■ ■111 ■' ■ ■ i ■ ■ ■ ■ i ■ ■ ■' i' •'11

Abundance 73 7.80 8.00 8.20 8.40 8.60 5000 m/z 45.03 10.16% 41 45

70 55 59 ■ ■ i "■ ■ i■ ■ • ■ i■ ■ ■ ■ i■■ ■ ■ i""i'1"i"'i"i i "'' i'" • i ■" ■ i “ ■11" " r ■ ■' i ■ “ ' i ■ ■" i1' m/z-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #763: 1-Butanamine, 3-methyl- 30 7.80 8.00 8.20 8.40 8.60 m/z 71.00 7.44% 5000

15 V 4144 55 58 70 87 nmmmm 1 ‘1' 11 ■ ‘1111111' "' 111'' I' ‘1111''' 1111 ‘ 1''1' 11''11'1111'1111 ■'' I'1 m/z-? 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 7.80 8.00 8.20 8.40 8.60

1227.D GCMS0208.M Thu Feb 21 09:31:50 2002 Page 1

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