GCMS analysis results for sample AD29782, Jan 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\DEC1401\29782.D Vial: 22 Acq On : 15 Dec 2001 11:00 pm Operator: 209 GALOS Sample : gems scan 12/10 a Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 1 N-Ethylformamide Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

7.60 3.82 ug/1 812095 1,4-Dichlorobenzene-d4 11.68

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 N-Ethyl formamide 73 C3H7NO 000627-45-2 9 2 1,3-Dioxolane, 2-methyl- 88 C4H802 000497-26-7 9 3 Pentane/ 3-methoxy- 102 C6H140 036839-67-5 9 4 1,3-Dioxolane, 2-(3-bromo-5,5,5-tri 352 C10H16BrC13O2 000000-00-0 9 Abundance Scan 278 (7.599 min): 29782.D (-) m/z 73.0.0 100.00% 73

5000 43 ............... 1 - 7.20 7.40 7.60 7.80 8.00 C I,I I 50 55 3? 67, J t.... 87 ..... 103 , । ■ ■ ■ ■ । < ■ • ■ । ■ T 110*10001—. ' 1 I ' m/z 42.95 27.31% m/z-> 10 20 30 40 50 60 70 80 90 100 110 — Abundance #292: N-Ethylformamide 30 73

5000 7.20 7.40 7.60 7.80 8.00 44 53 m/ Z 41.0,5 10.36%

m/z-> 15 i ' • • 10 20 J 30 40 I- K 50 _i 1 1 ' 1 i ■ ' ■ ■ i ' 60 70 80 ' • ■ i ' ■ 90 ■ ■ i ■ 1 1 1 100 110 i •

Abundance #62902: 1,3-Dioxolane, 2-methyl- 73 TTmr 7.20 T TIpnTm 7.40 7.607.80 8.00 5000 43 m/ z 44.9.5 10.02% 58 | 87 27 I ' 1 ' 1 I 1 ■ ' ■ i 1 ' ■ ■ I • — — । > ' 1 ■ I ■ ■ ■ ■ l • • 1 1 I > < 1 1 I1 -1 l I 1 m/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #1793: Pentane, 3-methoxy- 1 TT ' f 73 7.20 7.40 7.60 7.80 8.00 m/ z 71.00 7.02% 5000 45

27 33 39, 55 i • 1 ■ ■ i ' ■ ■ ' i ■ ■ ' ■ i 1 ' • m/z-> 10 20 30 40 7.20 7.40 7.60 7.80 BOQ 50 60 70 80 90 100 110

29782 .D GCMS1126 .M Fri Dec 28 13:12:25 2001 Page 1

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