GCMS analysis results for sample AE07505, April 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\APR18O2\75O5 .D Vial: 13 Acq On : 20 Apr 2002 5:18 am Operator: Sample : gc/ms scan 4/1 fb Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0419.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 1 N-Ethylformamide Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

8.11 0.33 ug/1 36533 1,4-Dichlorobenzene-d4 12.21 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 N-Ethyl formamide 73 C3H7NO 000627-45-2 9 2 Pentane, 3-methoxy- 102 C6H140 036839-67-5 9 3 1-Butanamine, 3-methyl- 87 C5H13N 000107-85-7 7 4 Formig acid, ethyl ester 74 C3H602 000109-94-4 5 Abundance 7. Scan 333 (8.105 min): 7505. D (-) m/ z 73.00 100.00% 73

5000 43 — I | I I | | | i r I I [ I I I I | I I i I |

7.80 8.00 8 20 8.40 11 I, , 55,....... । I । । ■ r1 1 1 ■ i 1 1 1 1 i 1 11 1 । 1 1 87 103 m/z 43.05 30.64% m/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #292: N-Ethylformamide 33 ...................... ................................. 73

5000 58 7.80 8.00 8.20 8.40 44 m/z 44.95 9.83% 15 ■ 1 i ' 1 1 1 i 1 —— 1 ' 1 ll 1111 i 1 ' 1 1 i 1 1 ■ 1 i 1 1 1 r i ■ 1 ■ ■ i 1 1 1 1 1 1 m/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #1793: Pentane, 3-methoxy-

5000 73 1 1 1 । 1 ‘ 1 ' i '

m/z 7.80 8.00 41.05 1. 8.20 1 1 i ' ' ■ 1 i 8.40 8.12% 45

m/z-> ■ ■ i 10 ' ■ ■ 1 । 1 20 41,33.39— 30 40 50 ' i 60 ' 55 ■ 1 1 ■ i ■1 70 80 ' ■ r1 1 1 ' i ■ ■ ' 1 i 1 1 1 '' I ' 1 ' 1 1 1 90 100 110 Abundance #763: 1-Butanamine, 3-methyl- ' 1 1 i 1 ' ■ 1 । ■ 33 7.80 8.00 8.20 8.40 m/ z 70.90 6.38%

5000

m/z-> 15 1 ■ i 1 ''' 1 i 1 1 10 20 30 i i 41I ,< । i | > 55 > [

40 50 70 70 87 — i | । i । i | । । i । । i i P । i i 1 i । i i i—i—।—r

60 80 90 100 110 ...... t........ 1 1 i 1 ‘ 1 1 i ' ‘ 1 1 i 1 1 1 ' i ' 1 1 ' I 7.80 8.00 8.20 8.40

7505.D GCMS0419.M Mon Apr 22 10:44:27 2002 Page 1

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