GCMS analysis results for sample AE01441, Mar 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C: \HPCHEM\1\DATA\FEB2102\1441.D Vial: 13 Acq On : 22 Feb 2002 1:55 am Operator: Sample : gc/ms scan 1/22 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 1 N-Ethylformamide Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

8.20 0.42 ug/1 33708 1,4-Dichlorobenzene-d4 12.34

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 N-Ethylformamide 73 C3H7NO 000627-45-2 9 2 Pentane, 3-methoxy- 102 C6H140 036839-67-5 9 3 3-Pentanol, 3-methyl- 102 C6H140 000077-74-7 9 4 1-But anamine , 3-methyl-____ 87 C5H13N 000107-85-7 7 Abundance ~/ ’Scan 344 (8.204 min): 1441 DC) m/ z 73.00 100.00% 1 73

5000 43 7.80 8.00 8.20 8.40 8.60 .......................... ,1. 51 ,.5.7........... ■ ■ i ■ • ■ ■ i ■ ■ • ■ i ■ ■ ■ 1 i 1 1 • ■ r’ .। , > । । i 111’I* ii 87 103 m/z 43.05 „ 28.99% m/z-> 10 20 __ 30___ 40____ 50___ 60____ 70 80 90 100 110 Abundance #292: N-Ethylformamide 30 73

5000 44 58 7.80 8.00 8.20 8.40 8.60 m/ z 41.05 11.35% 15 ■ ■ i ■ ■ ■ ' i ‘ | , ■ i ■ ■ ■ • i ■ ‘'l ■ i ■ ■ i ■ ■ ■ ■ i ' 1 ■ ‘ i ‘ ‘ ‘ ' i ■ ■ ' 1 1 1 1 1 1 1 1 miz-__ 10 20 30 40 50 60 70 80 90 100 110 Abundance 1/0m pentane, 3-rema 73 M ...M 8.00 8.20 8.40 8.60 7.80 5000 m/ z 44.95 10.87% 45

27 33 39 55 ' **III**IAIIIIIIIIIa1aIIIIIIII/IY* m/z-> _ 10 20 30 __ 40 50 60 70 80 __ 90 100__ 110 Abundance #63573: 3-Pentanol, 3-methyl- .... 73 7.80 8.00 8.20 8.40 8.60 m/z 71.00 5.72% 5000 55 27 45 87 | 39, 1 1. l । । । । । ■ ■ ' i ‘ ‘ ■ i ■ ' ■ ' i ' • 1 ■ i ■ ■ ■ ' i ■ ■ । ' i ■ 17411 1+’I t 1 ' I ' ' 1 1 I 1 1 m/z-> 10 20 30 40 50 60 70 80 90 100 110 7.80 8.00 8.20 8.40 8.60

1441.D GCMS0208.M Fri Feb 22 09:35:42 2002 Page 1

NYC-WTC_000009892