GCMS analysis results for sample AE03382, March 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\1\DATA\MAR0102\3382.D Vial: 46 Acq On 3 Mar 2002 8:36 am Operator: Sample gc/ms scan 2/4 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 N-Ethylformamide Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

8.19 3.46 ug/1 249954 1,4-Dichlorobenzene-d4 12.32

Hit# of 5 'entative ID MW MolForm CAS# Qual

1 N-Ethylformamide 000627-45-2 9 73 C3H7NO 2 Silane, tetramethyl- 000075-76-3 9 88 C4H12Si 3 1,3-Dioxolane, 2-(3-bromo-5,5,5-tri 352 C10H16BrC13O2 000000-00-0 9 4 1-Butanamine, 3-methyl- _ 87C5H13N 000107-85-7 7 Abundance Scan 343 (8.189 min): 3382.D (-) m/z 73.00 100.00% 73

5000 43 ' ■ i ■ ■

55 87 7.80 8.00 8.20 8.40 8.60 103 m/z~> 1, ■10P20.......... 1111, ___ 30 .....40___ 50 60 ■i■■11i'■■‘i' 70 80 , i 4r 90 100 110 120 m/z 43.05 28.65% Abundance ...... ........... #292: N-Ethylformamide 30 73

5000 44 58 7.80 8.00 8.20" 8.40 8.60 m/z 44.95 10.33% 15 | ———1 ■ ■ ।1 —T 1/a/a/t/1/441/aAaI*AIAPIIIIIII miz-> 10 20 30 40 50 60 _ 70 80 90 100 110 120 Abundance 73 ' । ‘ । ‘ ■ i ■ ■ ■ • i ■ ■ ■ ■ i ■ ■ 7.80 8.00 8.20 8.40 8.60 5000 m/z 41.05 10.07% 45 15 53 59 88 141 4,114 1 114/1 ***‘1 *‘ 1 * ‘ * * 1 ‘ ‘ 1 * 1 ***‘1‘‘‘‘I++‘‘I‘‘‘‘}‘*-‘I‘I mfz-> 10 20 _ 30 40 50 60 70__ 80 90 100 110 120 Abundance #49423: 1,3-Dioxolane. 2-(3-bromo-5,5,5-trichloro-2,2-dimet 73 7.80 8.00 8.20 8.40 8.60 m/z 71.00 7.11% 5000

45 36 55 ■ ■ i 1 • ■ ■ I 1 1 1 1 1 1 1 1 1 i I 67, 1 ' 1148’147 4 1' 1 1 + 108 115 ‘ i ' ■ ■ ■ i 1 1 1 1 1 1 ' 1 ' 1 1 m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 I 7.80 8.00 8.20 8.40 8.60

3382.D GCMS0208.M Mon Mar 25 12:22:24 2002 Page 2

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