GCMS analysis results for sample AE03382, March 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\1\DATA\MAR0102\3382.D Vial: 46 Acq On 3 Mar 2002 8:36 am Operator: Sample gc/ms scan 2/4 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 Divinyl sulfide Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

6.22 0.46 ug/1 32936 1,4-Dichlorobenzene-d4 12.32

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Divinyl sulfide 86 C4H6S 000627-51-0 36 2 2 - Pyrrol idinone 85 C4H7NO 000616-45-5 9 3 Methacrylamide 85 C4H7NO 000079-39-0 9 4 Oxirane,_ (2-methylpropyl) - 100 C6H120 023850-78-4 9 Abundance Scan 129 (6.224 min): 3382.D (-) m/z 84795 100.00% 85 41

5000

+ 60 .}iB ...... ........................................... 38 , 57 89 5.80 6.00 6.20 6.40 6.60 " i11 “ i11111" — 14' । 47 51 ■1 ” i1' ■ ■ i ■ ■' ■ i ■ ■ ■ • i ■ ■ • ■ i ■ ■ ■' 44 T-r-p-r m/z 41.05 70.36% m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #672: Divinyl sulfide 85

45 59 AA1A A/M MAM 5000 27 5.80 6.00 6.20 6.40 6.60 m/z 42.95 48.09%

m/z->__ 010 34 T-rp-n-rp- ''I' 'I11''I‘ "I'' P&mmm N/Ww. 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance 85

5.80 6.00 6.20 6.40 6.60 5000 42 m/z 39.0,5 33.12% 30 27 56 52 14+’1’AA*1**4*1t++*1**+41*4411+18+18//S2* m/z->_____ 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #618: Methacrylamide 85 .............. . 5.80 h , 6.00 -AA 6.20 6.40 6.60 41 m/ z 59.95 23.22% 44 5000 69

3E 53 all i‘ । “1' । ■ ..60,....^11... . +r 'i “ “ i“ I ‘ ' rr ■ ■ ■ ‘ I ■ ‘ ‘ ' I ‘ • m/z-> 20 25 30 35 40 45 50 55 65 70 75 80 85 90 95 5.80 6.00 6.20 6.40 6.60

3382.D GCMS0208.M Mon Mar 25 12:22:19 2002 Page 1

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