GCMS unknown compound report, Feb 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\l\DATA\FEB0802\30646.D Vial: 9 Acq On 8 Feb 2002 5:06 pm Operator: 209 GALOS Sample GC/MS SCAN 2/4 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 1,3-Dioxane Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

6.27 0.27 ug/1 26000 1,4-Dichlorobenzene-d4 12.35

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 1,3-Dioxane / 88 C4H802 000505-22-6 9 2 Methanethioamide, N,N-dimethyl- 89 C3H7NS 000758-16-7 9 3 Glycine, thyl ester 89 C3H7NO2 000616-34-2 9 4 2-(2,2-Dimethoxypropyl )-3-(methoxym 214 C11H18O4 087773-68-0 9 Abundance Scan 134 (6.275 min): 30646.D(-) m/ z 87.10 100.00% 87 43 55 5000 - 103 ____ 6.00 36 | . 1 71 - 6.20 6.40 _ 6.60____ " I" " I " " I" " J " ' I ' । I ! l! I i i । | i ri rH i i TIII | " P m/ z 89.00 ’ 86.15% m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 Abundance #808: 1,3 Dioxane 87

5000 31 dia ___ 6.00 6.20 6.40 6.60 m/z 71.01%

m/z-> ■" t ■ m 41 26 'I TITTTTTTTT 59 - 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 Abundance . 89 A-— 6.00 6.20 6.40 6.60 5000 m/z 55.00 55.40% 42 74 33 47 56 1'1' 1"1' i" " i" ■ ■ i" " i " " r " ■ i ■ ‘ ‘ r ■ " i " " i" " i " " r " ■ r ■ " r " ' i" ■' r "' i " " i" ' ‘ i" m/z--> . 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 Abundance #870: Glycine, methyl ester 89 -A. . ... 6.00 6.20 6.40 6.60 m/z 44.95 20.50% 5000- 44 59 mm iI ""I" 54 |, 66 "I"'1! ""I" i " " i' ■" i" " r '1 I " " r 1" r " ' i " ■ ■ i" m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 6.00 6.20 6.40 6.60

30646.D GCMS0208.M Mon Feb 11 12:30:05 2002 Page 1

NYC-WTC_000005191