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GCMS sample results, AE00916, Feb 26, 2002

Machine-extracted title · confidence 100%

Gas chromatography mass spectrometry results for sample AE00916 analyzed on February 26, 2002.

NYC-WTC_000009521–000009529

Folder label: “GCMS X 1/14/02 A 2/25-2/26

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\FEB1102\916.D Vial: 40 Acq On : 13 Feb 2002 2:05 am Operator: 209 GALOS Sample : GC/MS SCAN 1/14 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 2-Methyl-5-hexen-3-ol Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 8.23 0.35 ug/1 24029 1,4-Dichlorobenzene-d4 12.35 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 2-Methyl-5-hexen-3-ol 114 C7H140 032815-70-6 9 2 1,3-Dioxolane 74 C3H602 000646-06-0 4 3 Silane, tetramethyl- 88 C4H12Si 000075-76-3 4 4 Propane/ 2-methoxy-2-methyl- _____ 88 C5H120 ______ 001634-04-4 4 Abundance 7 Scan 347 (8.230 mln): 916.D (-) m/z 73.00 100.00% 73

5000 43

i ■ ‘ • i ■ ' ■ ' i ■ ‘ • ■ i • ' 7.80 8.00 8.20 8.40 8.60

miz-> T1 rm-rr l—51,5-444.RL l"'‘l" “I 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 , 86 11 “ “ I “ “ I ‘ “ I “ “ I' * m/z 43.05 44.33% Abundance #3017:2-Methyl-5-hexen-3-ol 73 55 43 .................. / 5000 1 * * *+1***1** 7.80 8.00 8.20 8.40 8.60 27 m/ z 41.0,5 18.22% 31

m!z~> i•■i‘■•■।■11“ “ i ‘ ...I.,,,..,,,, tmmh 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 H7l, +1 Abundance $62557 1,3-Dioxclane 73 l ■ ‘ ‘ ‘ i ■ * ■ ‘ i ■ ‘ ‘ • i ‘ • 29 44 7.80 8.00 8.20 8.40 8.60 5000 m/z 44.95 12.97% 15 19 26 11.... I.... 1111 ■ I11... 1. 1111.... I I! I n 11. WNPPTPPITPPTTITTEIIT 111111 mlz—> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #62932: Silane, tetramethyl- 73 7.80 8.00 8.20 8.40 8.60 m/z 71.00 7.90% 5000-

45 15 53 59 88 42 | THmpmm । .... j > > . . | . .. . । . . . 1 ( >, .. ।, .. . t ,।.!.I i ' 1 ■ • i * ■ ■ ■i■■11i i' ■ > । >> miz->5 10.15 2025 30 35 40 45 50 55 60 65 70 75 80 85 90 95 7.80 8.00 8.20 8.40 8.60

916.D GCMS0208.M Wed Feb 20 09:54:44 2002 Page 1

NYC-WTC_000009528

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NYC-WTC_000009528Source: NYC Law Department, mirrored locally

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