GCMS results for sample AE09654, May 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\1\DATA\MAY0602\9654.D Vial: 12 Acq On 7 May 2002 3:04 am Operator: Sample GC/MS SCAN 4/24 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0501.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 1-Propanesulfonic acid, methyl Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

6.26 2.62 ug/1 196735 1,4-Dichlorobenzene-d4 12.20

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 1-Propane s' fonic acid, methyl este 138 C4H10O3S1 002697-50-9 4 2 Hydrogen a zide 43 HN3 007782-79-8 4 3 3,8-Nonadien-2-one, (E) - 138 C9H140 055282-90-1 3 4 Methyl tert-butyl disulphide______ 136 C5H12S2 035166-82-6 3 Abundance f Scan 133 (6.257 min): 9654.D (-) m/z 43.00 100.00% 43

5000 ........ -..... 136 6.00 6.20 6.40 6.60 36 | 57 81 93 100 121 - m/z 42.15 11.69% ' 1 i 1 ' ' ■ i ' ' ' ' i ' ' ‘ 'T"+t 11 ।11 * 11 • i' 11 > । III ■ ■ ■ ।'' ■ 11 > > 111 । > > । । < । । 111 m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #6820:1-Propanesulfonic acid, methyl ester 43 / / 5000 ■ ■ 1 ■ । 1 ■7 ■ । ■ ■ ■ ■ । 1 1 ■ ■ । ■ 1 1 1

27 6.00 6.20 6.40 6.60 97 m/z 136.00 4.83% 59 79 107 ,................... i, , -PPPPPT -- TT1u0’I——138 In—r miz-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #33: Hydrogen azide 43 /w 6.00 6.20 6.40 6.60 5000 15 m/z 93.00 4.69%

29

■ ■ i' —PPPP 1 50 iao 70 80 90 100 110 120 130 140 mfz—> 10 20 30 40 Abundance #7007:3,8-Nonadien-2-one, (E)- W 43 6.00 6.20 6.40 6.60 55 m/z 138.00 4.56%

5000 95 80 67 123 ■ ■ i 1 ' r ' I 1 ‘ ' i ' ' ‘ ■ i ' ■ r ' i ■ 1 ■ ■ i ■ ■ ' • i' — i ' 1 '109 ,I 138 ' i ' ' ' ‘ i 1 ■ ■ ' i ' 1 1 ' i ' ■ ' ' I ' ‘ 1 ' I ‘ A ' 1 I ' ' ' ' I ' m/z—> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 6.00 6.20 6.40 6.60

9654.D GCMS0501.M Wed May 08 11:52:41 2002 Page 1

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