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GCMS analysis results for sample AE11379, May 28, 2002

Machine-extracted title · confidence 95%

Laboratory report documenting GCMS analysis of sample AE11379 conducted on May 28, 2002, including surrogate recovery data.

NYC-WTC_000025041–000025050

Folder label: “GCMS X 5/14/02 A 5/21/02

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NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C: \HPCHEM\ 1 \DATA\MAY2 102\11378.D Vial: 27 Acq On : 22 May 2002 2:23 am Operator: Sample : EXTRACTS/14 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0520.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 4-Penten-2-one, 4-methyl- Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 9.92 0.60 ug/1 38209 1,4-Dichlorobenzene-d4 12.14

Hit# of 5 / Tentative ID MW MolForm CAS# Qual ------------ - ------------------------- 1 4-Penten-2-one, 4-methyl- 98 C6H10O 003744-02-3 16 2 Acetic acid, 1-methylpropyl ester 116 C6H1202 000105-46-4 9 3 Methyl 1-methylcyclopropyl ketone 98 C6H10O 001567-75-5 7 4 2-Propanone, 1-cyclopropyl-______ 98 C6H10O 004160-75-2 5 Abundance ’ Scan 532 (9.916 min): 11378.D (-) m/z 43.05 100.00% 43

5000

58 87 1 ' ' 1 1 391 98 9.60 9.80 10.00 10.20

miz-> —H+ +49—4+ i1" ' i " " i mmTT m/z 69 83 ' i1" 11r' I I I I I I I I I I I I I I 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 58.10 21.74% Abundance #1244:4-Penten-2-one, 4-methyl- 43

5000 1 1 ' I ■ ' TIrrd/I/TI/TTTITLT 9.60 9.80 10,00 10.20 83 m/ z 87.05 17.16% 29 55 98 .................... .. HPTTTITT p mlz-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #3301: Acetic acid, 1 -methylpropyl ester 43 9.60 9.80 10,00 10.20 5000 m/ z 41.05 14.46% 56 87

m/z—> Abundance 29 61 73 - " I'1"101 -FHTTT 1TTTTTTTTTTTTTTHTTT 11" ‘ i " " I 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 #1241: Methyl 1 -methylcyclopropyl ketone 43 AMMMAAM,N.M,A./ m/z 9.60 j 9.80 10.00 10.20 59.10 12.48% 5000 55

27 83 98 - 1 1 ' " 50 , - 'l ' ' । 1 *T 1’"’’011211111111111111111’"7hi m/z—> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 9.60 9.80 10,00 10.20

11378.D GCMS0520.M Wed May 22 09:22:20 2002 Page 2

NYC-WTC_000025049

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NYC-WTC_000025049Source: NYC Law Department, mirrored locally

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