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GCMS analysis results for sample AE11602, June 2002

Machine-extracted title · confidence 90%

TCLP calibration table document dated May 24, 2002, listing deuterated standards and response factors for GCMS analysis.

NYC-WTC_000013943–000013967

Folder label: “GCMS X 5/24/02 A 5/28/02

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NYC 9/11 Public Portal Document Library Search Compound Report Data File : C: \HPCHEM\ 1 \DATA\MAY2 102 \ 116 02 . D Vial: 31 Acq On : 22 May 2002 8:06 pm Operator: Sample : EXTRACTS/20 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0520.M (RTE Integrator) . Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 Methyl Isobutyl Ketone Concentration Rank 6 R.T. EstConc Area Relative to ISTD R.T. 5.68 2.70 ug/1 173305 1,4-Dichlorobenzene-d4 12.15 Hit# Of 5 Tentative ID MW MolForm CAS# Qual 1 Methyl Isobutyl Ketone 100 C6H120 000108-10-1 . 2 2-Hexanone 100 C6H120 000591-78-6(50 3 2,4-Pentanedione 100 C5H802 000123-54-6 27 4 Acetone 58 C3H60 000067-64-1 9 Abundance Scan 69 (5.677 min): 11602.D (-) m/z 43.05 100.00% 43

5000 58 =EdRTTfTupmeuTguouu 85 100 5.40 5.60 5.80 6.00 48 53 67 72 '' “ I111' “ i ■' “ i1 +rrrTrp-rrrpr Ip.nTrtTlpn.pnipl" mmmmmmm m/z 58.1.0 34.02% n/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 Abundance #63351: Methyl Isobutyl Ketone 43

5000 1 58 5.40 5.60 5.80 6.00 27 m/z 41.05 19.58% 85 100

Ti/Z-> Tpuft -rrrp-m-p- '' 11 ''' I' ‘ ' I Z 1’10111001111110111 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #63387:2-Hexanone 43

58 5.40 5.60 5.80 6.00 5000 m/ z 57.10 18.21%

71 or 85 100 mmmmHmmmmmmmmmmpmm miz-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 Abundance #1473:2,4-Pentanedione 43 5.40 5.60 5.80 6.00 m/z 85.15 11.52% 5000 85 100 27 ,| , 37 | 53 58 72 T’’auu——00——mtmmmnpug miz—> 20 25 3035404550 55 6065 70 75 80859095 100 105 5.40 5.60 5.80 6.00

11602.D GCMS0520.M Fri May 24 08:33:06 2002 Page 1

NYC-WTC_000013948

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NYC-WTC_000013948Source: NYC Law Department, mirrored locally

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