NYC-WTC_000059172
Laboratory report documenting GCMS analysis of sample AE05235 for unknown compounds on April 9, 2002.
Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗Document / 16 pages
GCMS unknown compound analysis, sample AE05515, April 2002
Machine-extracted title · confidence 100%Laboratory record of gas chromatography mass spectrometry analysis for unknown compounds and surrogates on April 9, 2002.
NYC-WTC_000059317–000059332Folder label: “GCMS X 3/11/02 A 4/1/02”
Page image
OCR text
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report
Data File C:\HPCHEM\1\DATA\APR0102\5515.D Vial: 6 Acq On 1 Apr 2002 4:11 pm Operator: Sample gc/ms scan 3/11 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 4-O-Acetyl-2,5-di-O-methyl-3,6 Concentration Rank 6
R.T. EstConc Area Relative to ISTD R.T.
7.28 0.76 ug/1 128362 1,4-Dichlorobenzene-d4 12.25
Hit# of 5 Tentative ID MW MolForm CAS# Qual ___________ i____________ 1 4-0-Acet -2,5-di-O-methyl-3,6-dide 215 C10H17NO4 000000-00-0 38 2 2-Pentan 1, 2-methyl- 102 C6H14O 000590-36-3 38 3 4-Penten -2-ol, 2-methyl 100 C6H12O 000624-97-5 36 4 2-Prop^^ol, 2-methyl- 74 C4H10O 000075-65-0 36 iAbundance~ ■ “ Y ....... . .... 2^ (7.283 miti): 5515.D (J m/z 59.05 100.00% 50
5000 43
107 _____j U-r ... . 51 •tWn* 87 I, 71 I'' '■ I I'''' I I " '»I • 11.111 m/z 7.00 7.20 43.05 7,40 7.60 44.43% m/z-> 10 20 30 40 50 60 70 801 90 100 110 120 130 140 150 160 170 Abundance #26486: 4-O-Acetyl-2,5-di-O-methyl-3,6-dideoxy-d-gluconitri I 50
“Or1 i-n , , I > I I I ,T-i ri' 5000 43 7.00 7.20 7.40 7.60 m/z 41.00 18.05% 71 97 113 156 173 I Tfr '''' I' ‘ j''''I > I.. I '' ' I' I'' ’' I ’' !m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 Abundance #63532; 2-Pentario!. 2-methyl- 59
7.00 7.20 7.40 7.60 5000 m/z 107.00 15.20% 45 87
I 3-' ! 69 I'''' I' '' ‘ I'''' I''' ■ I' ' I 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 /abundance #1529: 4-Pentene-2-ol, 2-methyl ... A 7.00 7.20 7.40 7.60 m/z 71.00 6.07% 43 5000
31 js, ,1 y ' I' 6.7 '85 I " »’ pr^ny PTTry I'''' I ‘' I'''' I A........ A, I, .Y]........... im/z--> 10 20 30 40 50 60 70 80 90100110 120 130 140 150 160 170 TOO 7.20 7.40 7.60
5515.D GCMS0403.M Thu Apr 04 13:52:55 2002 Page 2
NYC-WTC_000059325
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NYC-WTC_000059325Source: NYC Law Department, mirrored locally
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