TCLP calibration table review document, April 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\APR1202\8481.D Vial: 26 Acq On : 16 Apr 2002 9:08 am Operator: Sample : gc/ms scan 4/10 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 1 3-Penten-2-one Concentration Rank 4 R.T. EstConc Area Relative to ISTD R.T. 5.76 0.90 ug/1 128312 1,4-Dichlorobenzene-d4 12.23 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3-Penten-2-one 84 C5H80 000625-33-2/86 ) 2 3-Penten-2-one, (E)- 84 C5H80 003102-33-883/ 3 2-Pentene, 4-methyl-, (Z) - 84 C6H12 000691-38-3 72 4 2-Pentene, 2-methyl-____________ 84 C6H12 000625-27-4 64 Abundance Scan 78 (5.759 min): 8481 .D (-) m/z 69.00 100.00% 69 41

5000 84 ■ ■ i ■ ■ ’dT 1 I 1 38 5.40 5.60 5.80 6.00 6.20 | 14 47 50 53 61 66 t i n । i i | > i । । | i n i n I I r I । । r। i i j 1 । I । । । । । i । i i i । [ i i 1 r 1 1 11 ■ ■1 11 1 11 1111' I m/ z 41.05 72.60% m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 Abundance #62734:3-Penten-2-one 69

41 5000 T71 5.40 5.60 5.80 6.00 6.20 84 m/z 42.95 43.70% 27 383 । 14 55 i । j t i i i ~| -rt—। । । । । i । । । I- 1 1 111 11 111' ■ ■ i ■ ■ - ■ ।r ■ ■ -11 ■ - 111 ■ 1 11 1 11 11 ■' ■ i11 1 11 m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 Abundance #564: 3-Penten-2-one, (E)- 41 69 TTTTTuunuummumTT 5.40 5.60 5.80 6.00 6.20 5000 m/z 39.05 34.26% 84 27 38 T 111 111 r 1111 n 111 r 49 53 | 1 1 | 1 1 | ' 1 1 । | । । 1 I | I I ! I | ‘1 i1 11'111 11 । I । j “ । । r । । i । r i । । । m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 Abundance #601: 2-Pentene, 4-methyl-, (Z)- —4T Al 41 69 5.40 5.60 5.80 6.00 6.20 m/ z 83.90 31.48% 5000 84 27 53 56 37 I ! - I I I ! | ! > -'I | । — 65 , ' I' ' ' 1 1 TTmnp"1 ■ -1 ■ ■ ■ ■ i ■ • 11r'1I '1 1 1I 1 1 I 1 ' 1 ' 1 1 ' 1 1 I ' ' ‘ 'T' 1 1 I 1 m/z—> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 5.40 5.60 5.80 6.00 6.20

8481.D GCMS0412.M Fri Apr 26 12:47:20 2002 Page 1

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