GCMS analysis results for sample AE06455, April 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\APR1702\6455.D Vial: 13 Acq On : 17 Apr 2002 7:57 pm Operator: Sample : gc/ms scan 3/19 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L Peak Number 2 2-Pentene, 2-methoxy- Concentration Rank 14 R.T. EstConc Area Relative to ISTD R.T. 8.25 0.40 ug/1 46716 1,4-Dichlorobenzene-d4 12.21 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Pentene/ 2-methoxy- 100 C6H120 061142-47-0 22 2 2,7-Octanedione 142 C8H14O2 001626-09-1 9 3 1 -Hexadecanol 242 C16H34O 036653-82-4 9 4 2-Propanone, 1,1,1-trichloro- 160 C3H3C130 000918-00-3 9 Abundance Scan 349 (8.247 min): 6455.D () m/z 43.05 100.00% 43

5000

' 1 1 1 I 1 1 1 1 I 1 ' 1 1 I ' f ' 1 I 1 8.00 8.20 8.40 8.60 ................ ] I I I ’ > [ di! t,! .5 59 72 83 97 I | .I I 7 1 ,,11I 1 I 1 ...It ................ ................... I | I I I I I I I I ! 125 | I I I I | I ! I 1 ................... | T ! 1 1 ] I I I •I | 1 T m/z 124.75 10.57% miz-> 20 40 60 80 100 120 140 160 180 200 220 Abundance #1570: 2-Pentene, 2-methoxy- 43 55 72 85

5000 —. . i > । i . . . । , ri . । , 1 1 1 1 ' 100 8.00 8.20 8.40 8.60 m/z 82.85 8.24% 111 1 ' 1 ' 1 I ‘ ' 1 1 ' ' i ‘ ' m/z-> 20 40 60 80 100 120 140 160 180 200 220 Abundance #7959: 2,7-Octanedione 43 ■ 1 । ' ' 1 ■ i ■ ■ ■ 8.00 8.20 8.40 8.60 5000 m/z 96.95 5.98% 84 58 71 - 99 114.......... 142..................................................... m/z-> 20 40 60 80 100 120 140 160 180 200 220 Abundance #71247:1-Hexadecanol 43 8.00 8.20 8.40 8.60 55 m/z 98.85 5.33% 5000 83 27 70 97

i ' ' 1 1 i ' 1 II 1TI _ 111 1. 125..... 1 i ■ I । i I । । ' । I । 1 ■ ■ i ■ ■ ■ ■ i ■ • • । i ■ ■ ■ ■ । । 1 196 224 m/z—> 20 40 60 80 100 120 140 160 180 200 220 8.00 8.20 8.40 8.60

6455.D GCMS0412.M Thu Apr 18 09:14:13 2002 Page 2

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