GCMS analysis results for sample AE08686, April 26, 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\APR2202\8686.D Vial: 8 Acq On : 22 Apr 2002 4:01 pm Operator: Sample : gc/ms scan 4/11 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 2-Pentanone, 4-hydroxy-4-methy Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T.

8.19 6.58 ug/1 776533 1,4-Dichlorobenzene-d4 12.21

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 2-Pentanone, 4-hydroxy-4-methyl- 116 C6H12O2 000123-42-2 40 2 CH2=CHCH2C(O)OCH3 100 C5H802 003724-55-8 10 3 Butane 1-ethoxy- 102 C6H140 000628-81-9 9 4 5-Hexe -2-one 98 C6H10O 000109-49-9 9 Abundance V Scan 343 (8,192 min): 8686.D (-) m/z 43.00 100.00% 43

59 5000 101 1441“r 8.00 8.20 7.80 8.40 8.60 T’T’’ .... .. 53 . ip ■ r ■ "I . ....... 71........83........... 1 WIPBgur m/z 59.05 52.72% mz—> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 110 Abundance #64274:2-Pentanone, 4-hydroxy-4-methyl- 4)3

5000 59 7.80 8.00 8.20 8.40 8.60 m/z 101.05 22.24% 27 . 101 q +49+H l“ i“■•i•• i 83 i “1 • i ■ ■ “ । “i“ I ■i , i ThT miz-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 Abundance #1448: CH2=CHCH2C(O)OCH3 43 * । * • * * । ■ * 7.80 8.00 8.20 8.40 8.60 5000 m/z 58.05 16.82%

58

miz-> । ‘। 3, +720 WRTUTTETRTTT1’1’111111+111177911111191303"0"TTITE1 ’r 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 Abundance #63550: Butane, 1-ethoxy- ■ i ■ ■ ■ ■ i ‘ • 50 7.80 8.00 8.20 8.40 8.60 31 m/ z 41.00 7.43%

5000

73 I 87 102 11 ■1 ■ i ■"' i"' ‘ i ■ ■ ■ ■ i''" i ‘1" i" “ i “'11'1 ■ ■ i •11 ■ i ■ • *Tfdn—mmeOTRuu!rt miz-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105110 7.80 8.00 8.20 8.40 8.60

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