GCMS analysis results, sample AE05057, April 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\MAR3002\5057.D . . Vial: 33 Acq On : 31 Mar 2002 12:42 am Operator: Sample : gc/ms scan 3/8 fb Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 1 3-Penten-2-one, 4-methyl- Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

7.18 0.34 ug/1 45368 1,4-Dichlorobenzene-d4 12.25

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3-Penten-2-one, 4-methyl- 98 C6H10O 000141-79-7 /'91A 2 2-Pentene, 2,4-dimethyl- 98 C7H14 000625-65-0 ^9.1J 3 2-Pentene, 3,4-dimethyl-, (E)- 98 C7H14 004914-92-5 78 4 2-Pentene, 4,4-dimethyl-, (E)- 98 C7H14 000690-08-4 ____ 78 Abundance Scan 232 (7J78 min): ’5057.0 (-) 55 8b

5000 43 98

3^ I, 50 , 6.80 7.00 7.20 7.40 7.60 p"'I""I •1T.T|-I.jlllllllll..|hll I "' I" " I" '' I' "' I"'' I" m/z 55.00 86.60% m/z-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 Abundance #63217: 3-Penten-2-one. 4-methyl- 5o 8i3

43 98 I 5000 i I I 6.80 ■ 1 ■ ■ 7.00 7.20 7.40 7.60 i m/z '^^•95 ' 43.56% I. I 50 67 5 10 15 20 25 30 35 40 50^ 60' 65" 70' 75' 80 85 90" 95' 100 'l OS^. Abundance ;;G3271: 2-Pertae, 2,4-diT’e;hyl- 55 83

6.80 7.00 7.20 7.40 7.60 m/z 97.95 42.10% 5000 41 98 a 27 •50 67 TTTrrpYTTpn-rryrrrrp-TTT^^ TTTrrpTTTpTTTJTTT^ ' I' "' I" " m/z-> 5 10 15 20 25 JO 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 Abundance #1362: 2-Pentene, 3,4-dimethyl-, 56 43 "Tso^ 7.00 7.20 7.40 7.60 m/ z 24.72% 5000 27 98 15 ........... I'l.............|HH|.ill|lliq9ill|llH|-|lll|li.l|l,l,|U.I|Tri4|riTt|UU|HII|................ /\/\A A m/z-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 6.80 7.00 7.20 7.40 7.60

5057.D GCMS0308.M Tue Apr 02 15:34:58 2002 Page 1

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