GCMS analysis results, sample AE05057, April 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\MAR3OO2\5O57.D Vial: 33 Acq On : 31 Mar 2002 12:42 am Operator: Sample : gc/ms scan 3/8 fb Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 Butane, 2-methoxy-2-methyl- Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

8.14 0.62 ug/1 82749 1,4-Dichlorobenzene-d4 12.25

Hit# of 5 Tentative ID MW MolForm CAS# . Qual 1 Butane,/2-methoxy-2-methyl- 102 C6H14O 000994-05-8 33 2 Pentane, 3-methoxy- 102 C6H14O 036839-67-5 28 3 1,3-Dyoxolane, 2-(3-bromo-5,5,5-tri 352 C10H16BrC13O2 000000-00-0 9 4 1-ButAnamine, 3-methyl-__ _ ______ 87 C5H13N _000107-85-7 7 Abundance ......... " Scan 337 (8.142 mirij: 5057.D m/ z 73.00"” i66"7oo% 43

5000 43

I, 50^ 65....• I 87 7.80 _8.2^J3.^____ 71-'-.......... -"‘Jl 103 t-r I ' ' A I m/ Z 43.05 29.76% m/z-> 20 30 40 50 60 70 80 90 100 110 120 Abundance #1761: Butane, 2-niethoxy-2-methyl-

I 5000 ........... 7.80 8.00 8.20 8.40 __ 55 87 I m/ z 41.05, 11.54% 2,^' 33. 45I I I T-f-T—I—r-r iTl/Z-> 20 30 40 50 60 70 80 90 100 110 120 Abundance i"!793 Pentane, u-metboxy- 73

7.80 8.00 8.20 8.40 5000 m/z 44.95 11.22% 45

. ... Ik , 27 33 39 55 m/z-> 20 30 __ 4p___ 50 60 7Ci 80 90__ 100 110__ 120 Abundance #49423: 1,3-Dioxolane, 2-(3-bromo-5,5,5-trichioro-2,2-dimet 1 7)3 7.80 8.00 8.20 8.40 i m/z 7.64%l 5000

I 45 I 3,6 , I I 55 ............................... 109114 20 30 40 50 60 70 80 90 100 110 120 7.80 8.00 8.20 8.40

5057.D GCMS0308.M Tue Apr 02 15:35:03 2002 Page 2

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