GCMS analysis results, sample AE05057, April 2002

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Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\MAR3002\5057.D Vial: 33 Acq On : 31 Mar 2002 12:42 am Operator: Sample : gc/ms scan 3/8 fb Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 3 2-Pentanone, 4-hydroxy-4-methy Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

8.22 1.64 ug/1 220522 1,4-Dichlorobenzene-d4 12.25

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 2-Pentano/e, 4-hydroxy-4-methyl- 116 C6H12O2 000123-42-2 64 2 Acetic acid, 1,1-dimethylethyl este 116 C6H12O2 000540-88-5 28 3 5-Hexen-/2-one 98 C6H10O 000109-49-9 12 4 CH2=CHCg2C(O)OCH3 100 C5H8O2 003724-55-8 10 Abundance Scan 346 (8.224 min): 5057.D (-) m/z. 4 3‘;oo. ..lOOTd^ 4(3

5000 59

101 83 7.80 8.00 8.20 8.40 8.60

m/z->__ . ............. 38 I 1 ' ' ' ' I ' ' ‘ ' I ' ' ' ' 1 ' 10 20 30 40 50 I'll60..... n70 80 I 90 I I ' ' ' ' I 100 110 m/z 59.05 47.99% Abundance #64274: 2-Penlanone, 4-hvdroxy-4-methyl- 4l3

5000- 59 7.80 8.00 8.20 8.40 8.60 m/z 101.05 21.46% 27 101 I 49 83 I 'm/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #3292; Acetic acid. 1.1-d:me‘iiyl<:'nyi ester 4'3 ...................... 7.80 8.00 8.20 8.40 8.60 5000 57 m/z 15.16% 101 15 27 m/z-> 10 20 30 40 50 60 70 80 90 100 1W Abundance #63205: 5-Hexen-2-one I 40 7.80 8.00 8.20 8.40 8.60 m/z 83.05 7.04% 5000

55 15I VI 38 , 50 I 83 98 .... , m/z-> 10 20 30 40 50 60 70 80 90 100 110 7.80 8.00 8.20 8.40 8.60

5057.D GCMS0308.M Tue Apr 02 15:35:07 2002 Page 3

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