GCMS calibration results for sample AE09585, May 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\l\DATA\MAY0302\9585.D Vial: 12 Acq On 4 May 2002 12:49 am Operator: Sample GC/MS SCAN 4/24 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0501.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 1 2-Pentanone, 4-hydroxy-4-methy Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

8.16 12.77 ug/1 818261 1,4-Dichlorobenzene-d4 12.20 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Pentanone, 4-hydroxy-4-methyl- 116 C6H1202 000123-42-2 64 2 CH2=CHCK2C(O)OCH3 100 C5H802 003724-55-8 9 3 Acetone 58 C3H60 000067-64-1 7 4 5-Hexen-2-one 98 C6H10O 000109-49-9 5 Abundance Scan 340 (8.156 min): 9585.D (-) m/ z 43.05 100.00% 43

5000 59 11* —n i^iji । 101 7 80 8.00 8.20 8.40 8.60 i 1 1 ■ ■ i ' 1 1 ' i ' 1 1 38' i I ■ -453...ff5 I i । —69 83 | । 1 । “i" > । ~> ' । i i TT । I । r i i j । r m/z 59.10 42.19% m/z-> 10 20 30 40 50 I60 70 80 90 100 110 Abundance #64274: 2-Pentanone, 4-hydroxy-4-methyl- 43

5000 59 780 8.00 8.20 8.40 8.60 m/z 58.10 15.85% 27 101 .......40 +49+ 83 m/z-> 1.......... 10 20 1, 30 50 60 ' I ' ' ' ■ i ' 1 ■ 1 i 1'1 ' ' i ' 70 80 90 —1-- i ' 100 110 Abundance #1448: CH2=CHCH2C(O)OCH3 43 7.80 8.00 8.20 8.40 8.60 5000 m/z 101.15 13.02%

58 .................... 38 1— ' i 1 1 1 1 1 72 i ■ ’ ■ 1 i 1 1 1 ■ i 1 100 1 I 1 1 1 1 I 1 1 1 ' 1 1 1 1 ' 1 1 m/z- > 10 20 30 40 50 60 70 80 90 100 110 Abundance #94: Acetone 43 7.80 8.00 8.20 8.40 8.60 m/ z 41.10 7.16% 5000 15 58 27

m/z-> — 10 4 ' । 1 1 1 1 । 1 1 1 1 । 1 1 ■ * । 1 1 20 30 40 50 60 70 80 90 100 110 r 1 1 > । i । । । i । । ii । TT") । । ।•

7.80 8.00 8.20 8.40 8.60

9585.D GCMS0501.M Mon May 06 10:50:43 2002 Page 1

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