GCMS analysis report for sample AE09452, May 2002

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Library Search Compound Report

Data File C:\HPCHEM\1\DATA\MAY0202\9452.D Vial: 17 Acq On 3 May 2002 6:38 am Operator: Sample GC/MS SCAN 4/22 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0501.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 1 2-Pentanone, 4-hydroxy-4-methy Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

8.16 13.47 ug/1 882668 1,4-Dichlorobenzene-d4 12.19

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2 - Pentanone , 4-hydroxy-4-methyl- 116 C6H1202 000123-42-2 78 2 CH2=CHCH2C(O)OCH3 100 C5H802 003724-55-8 9 3 Acetone 58 C3H60 000067-64-1 7 4 5-Hexen-2-one 98 C6H10O 000109-49-9 5 Abundance / Scan 341 (8.161 min): 9452.D (-) m/z 43.05 100.00% / 43

........... _ 5000 59

l il 1 1 1 1 1 "1 1 1 1 1 I I I I 1 1 I I I- 101 7.80 8.00 8.20 8.40 8.60 38 I 53 , 69 83 | ' 1 I 1 Bi । । r ■ । ■ i । । i i । । । । । i । i‘i i । । । । । 1’4 । । । । r m/z 59.10 42.66% m/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #64274: 2-Pentanone, 4-hydroxy-4-methyl- 43

5000 59 7.80 8.00 8.20 8.40 8.60 m/z 58.10 16.11% 27 101 83 — ... I,130... 49— I ' 1 1 1 i 1 1 1 ■' i 1 1 i । । ■ ■ 1 ■ । - m/z-> 10 20 40 50 60 70 80 90 100 110 Abundance #1448: CH2=CHCH2C(O)OCH3 43 r 1 i 1 1 1 1 । 1 1 1 1 r 1 ~i ' J 1 1 i 1 7.80 8.00 8.20 8.40 8.60 5000 m/z 101.15 13.18%

3? 1 58 72 100 ■ I ' 1 ' ■' I ' ' ' ' I I ' ' 1 I ■ 1 ' ' I ' I ' ' I I 1 I I I 1 m/z--> 10 20 30 40 50 60 70 80 90 100 110 Abundance #94: Acetone 43 7.80 8.00 8.20 8.40 8.60 m/ z 41.10 6.97% 5000 15 58 27 1 । । । ।' I । । ] । — r । । । ‘ । * I । । । । 7 । : । । । । - r* 1,1.11 ’ |—i-, । > । । । । । । i r-1-r-| i i i i । । m/z--> 10 20 30 40 50 60 70 80 90 100 110 7.80 8.00 8.20 8.40 8.60

9452.D GCMS0501.M Fri May 03 12:23:29 2002 Page 1

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