GCMS calibration results for sample AE09580, May 2002

NYC 9/11 Public Portal Document

Library Search Compound Report Data File C:\HPCHEM\l\DATA\MAY0302\9580.D Vial: 10 Acq On 3 May 2002 10:51 pm Operator: Sample GC/MS SCAN 4/24 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0501.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L Peak Number 1 2-Pentanone, 4-hydroxy-4-methy Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T. 8.16 13.48 ug/1 926112 1,4-Dichlorobenzene-d4 12.19 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Pentanone, 4-hydroxy-4-methyl- 116 C6H12O2 000123-42-2 64 2 3-Hydro: y-2-pentanone 102 C5H10O2 003142-66-3 9 3 CH2=CHC 2C(O)OCH3 100 C5H802 003724-55-8 9 4 5-Hexen 2 - one 98 C6H10O 000109-49-9 7 Abundance Scan 340 (8.158 min): 9580.D (-) m/z 43.05 100.00% 43

5000 59

1 ' i 1 1 1 । । i— I । । । । i T । । । r i । i 101 7.80 8.00 8.20 8.40 8.60 ................ 38 I 53 , 69 77 83 | 1 I I I I ! I I I 1 I I I I I I I I I +1+ | ! f I I | I I I 7 [ I I I I | I I I I | I T f I | | m/ z 59.10 43.43% m/z--> 10 20 30 40 50 60 70 80 90 100 110 Abundance #64274: 2-Pentanone, 4-hydroxy-4-methyl- 43

5000 1 ‘ i 1 ' ' _____ ____ _ _______ 1 l‘ 1 1 ‘ I 1 1 I 1 1 ' 1 I ' 59 7.80 8.00 8.20 8.40 8.60 m/z 58.10 16.25% 27 101

m/z-> 10 20 I I 30 FT 40 4950—+ 60 '

70 I

80 ■ 1 1 ■ i 1 1 1 ■ I ■11 83 ■ ' i 90 4 7 .11 100 110 Abundance #1691:3-Hydroxy-2-pentanone 31 59 ~' ■ i 1 ' 1 1 i ■ 1 1 1 i ' ' i r 1 1 1 I 1 780 8.00 8.20 8.40 8.60 5000 m/z 101.15 13.88% 45 15 l N I । ' 1 1 । 1 I . ,6.6. 73.. 84. 102 m/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #1448: CH2=CHCH2C(O)OCH3 — 43 7.80 8.00 8.20 8.40 8.60 m/z 41.05 6.93% 5000-

m/z-> 10 ........... . 20 30 40 —.. ff -..72 50 60 70 ■

80 i ■ ■ ■ •

90 1 ■ ■ ■ 1(X) -

100 | ■ 1

110 I । । । 7.80 iii-।

8.00 pr ii । । i । । । |“i । । । । r 8.20 8.40 8.60

9580.D GCMS0501.M Mon May 06 10:50:13 2002 Page 1

NYC-WTC_000046281