GCMS calibration results for sample AE09586, May 2002

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Data File C:\HPCHEM\1\DATA\MAY0302\9586.D Vial: 13 Acq On 4 May 2002 1:48 am Operator: Sample GC/MS SCAN 4/24 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0501.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 1 2-Pentanone, 4-hydroxy-4-methy Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T. 8.17 17.50 ug/1 1066330 1,4-Dichlorobenzene-d4 12.20 Hit# of Tentative ID MW MolForm CAS# Qual

1 2-Pentanone, 4-hydroxy-4-methyl- 116 C6H12O2 000123-42-2 64 2 CH2=CH(£H2C (O) OCH3 100 C5H802 003724-55-8 9 3 Acetone 58 C3H60 000067-64-1 7 4 5-Hexen-2-one 98 C6H10O 000109-49-9 7 Abundance Scan 341 (8.165 min): 9586.D (-) m/ z 43.05 100.00%| 4

5000 59

1 ' | 1 I > I | I I Tl | I I I "I | I I I L T” I 101 7 80 8.00 8.20 8.40 8.60 ....................................... 3? I 11 53.,J . PT 69 83 . | i । i i i i । ri < i । i i i—t' d i' i i । r m/z 59.10 42.23% m/z—> 10 20 30 40 50 60 70 80 90 100 110 Abundance #64274: 2-Pentanone, 4-hydroxy-4-methyl- 43

5000 59 7 80 8.00 8.20 8.40 8.60 m/z 58.10 16.52% 27 101

m/z--> I ■■ r ' pHl,.. । I 10 20 30 40 +49+ 50 60 83 I 1 1 1 1 I ' 1 ' ' i ''' 1 1 i 70 80 90 + 100 110 Abundance #1448: CH2=CHCH2C(O)OCH3 43 । । । । । । । । IEu । । । i ri । । i r-1 । 1 f 7 80 8.00 8.20 8.40 8.60 5000 m/z 101.15 13.55%

58 ........ 38, 1 72 100 m/z-> । 1 < । । । 1 ■ * * । 1 1 ' 1 I 10 20 30 40 1 50 60 70 0* 80 90 100 110 Abundance #94: Acetone 11’11 * 1 ‘ ‘‘ I >-TT| i-I i i । , 43 7 80 8.00 8.20 8.40 8.60 m/z 41.10 7.06%

5000 15 58 27 1 ........... .. ' ' ' 'Tl 1 ' i ■ ■ TI"III i I *T 1"^ I ] I PT | | 11 (| T T ' m/z-> 10 20 30 40 50 60 70 80 90 100 110 7.80 8.00 8.20 8.40 8.60

9586.D GCMS0501.M Mon May 06 10:50:57 2002 Page 1

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