GCMS calibration results for sample AE09586, May 2002

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Data File C:\HPCHEM\1\DATA\MAY0302\9586.D Vial: 13 Acq On 4 May 2002 1:48 am Operator: Sample GC/MS SCAN 4/24 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0501.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 Cyclopentasiloxane, decamethyl Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T. 14.80 2.13 ug/1 164668 Naphthalene-d8 15.83 Hit# Of 5 Tentative ID MW MolForm CAS# Qual 1 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 (80 2 3,4-DihydrQSxybenzyl alcohol, tris (tr 356 C16H3203Si3 068595-79-9 47 3 Phenethylami ne, N-methyl-.beta.,3,4 399 C18H37NO3Si3 010538-85-9 38 4 Benzenee anamine, N-[(pentafluorop 475 C21H26F5NO2Si2 055429-85-1 37 Abundance / Scan 1065 (14.799 min): 9586. D (-) m/ z 73.10 100.00% 73

5000 267 355 ,......... 45 1440 14.60 14.80 15.00 15.20 103118133 154 177 193 223 L 323339 m/z 355.10 i | i i i i | | ।i r [ ( i ' I " '11'1'' 'I' i i| i i ( i [ i i i ( |r7i i | Ini | i I ii | i i i i | i i i i | 36.39% m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #51266: Cyclopentasiloxane, decamethyl- 73

355 267 5000 0 14.40 14.60 14.80 15.00 15.20 m/z 267.05 35.92% 323339 1 191 207 •p-TT-T-p-Y-T-q- 251 I TPITT 1 T1 1 1 1 I ' ■ ■" I 1 1 "TUT !’’ ’ T ’ ’ Tr m/z~> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #49868: 3,4-Dihydroxybenzyl alcohol,tris(trimethylsilyl)- 73 । i I i i [ i i i / ] \ i i i । i i । i । r r

14.40 14.60 14.80 15.00 15.20 267 m/Z 356.10 13.25% 5000 179 356 45 147 i j i 1 . i i i [ i i 209 237 , l r i | > < 312 341 | । 1 1 । | । । ' tpT It i r t . p < i i । > i i i । i i i i । TT‘ i i i i । i TH 1’Y411dguui m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #74239: Phenethylamine, N-methyl-.beta.,3,4-tris(trimethyls ................. [ I I I I \ I I I I -f I I I I I I I I I I I I I

73 14.40 14.60 14.80 15.00 15.20 m/ z 2 68.05 9.04%

5000 355 fl 44 267 294 11171170/88 193 130147 ' [ । । ' । । । । i‘ । । । * । । । । । । I | i i i i i "i i' i । i i । i । 'i 7 t i । i i i i । i i i i । i i r i [ i ................. \........................ m/z—> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 14.40 14.60 14.80 15.00 15.20

9586.D GCMS0501.M Mon May 06 10:50:58 2002 Page 2

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