GCMS calibration table data, sample AE09519, May 2002

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Calibration table listing response factors for deuterated standards and target compounds used in gas chromatography-mass spectrometry analysis.

NYC-WTC_000013146–000013153

Folder label: “GCMS X 5/21/02 A 5/21/02”

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NYC 9/11 Public Portal Document Library Search Compound Report Data File C:\HPCHEM\1\DATA\MAY0 302\9519.D Vial: 20 Acq On 4 May 2002 8:41 am Operator: Sample GC/MS SCAN 4/22 Inst : 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0501.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 Cyclopentasiloxane, decamethyl Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 14.80 1.16 ug/1 110095 Naphthalene-d8 15.82 Hit# of 5 /Tentative ID MW MolForm CAS# Qual 1 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6(80 2 3,4-Dihydrpxybenzyl alcohol,tris(tr 356 C16H3203Si3 068595-79-9 43 3 Benzoic acid, 2,4-bis[(trimethylsil 370 C16H30O4Si3 010586-16-0 37 4 Phenethylamine, N-methyl-.beta.,3,4 399 C18H37NO3Si3 010538-85-9 37 Abundance Scan 1065 (14.797 min): 9519. D (-) m/z 73.05 100.00% 73

5000 267 .................... )....................... 355

45 14.40 14.60 14.80 15.00 15.20 i । 108 133 154170 193 223 251 । li 323339 1 414 “ * i TTTTRTmOPTDlaaapaaaandhanad/ ’ 1 m/z 267.05 34.87% m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #51266: Cyclopentasiloxane, decamethyl- 73

355 267 5000 14.40 14.60 14.80 15.00 15.20 m/z 355.10 32.30% 191207 323339 | 251 I ‘I 14 ‘ 1‘ 11 '' ’ I " * ‘ I ‘1'' I i ■ "ni 1 ■ i'" ‘1" '^i p-rT-rpr-rrT-j- m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #49868:3,4-Dihydroxybenzyl alcohol,tris(trimethylsily!)- 73

14.40 14.60 14.80 15.00 15.20 5000 267 m/z 356.10 12.74% 179 356 45 147 I , _27 ■।■■ 209 .312 1T7.1 L j > । > 11 < 111111 • i f > < 11") > <., । mz-> 40 60 80 1(X) 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #73975: Benzoic acid, 2,4-bisI(trimethylsilyl)oxy]-1 trimet 73 14.40 14.60 14.80 15.00 15.20 m/z 268.05 9.31% 5000 355 45

+++133149 — 193 22321-30 370 ‘ ‘11 * i • * • * । * ■ 1 T miz--> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 14.40 14.60 14.80 15.00 15.20

9519.D GCMS0501.M Tue May 07 09:38:29 2002 Page 2

NYC-WTC_000013152

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NYC-WTC_000013117

Calibration table listing response factors for deuterated standards and target compounds used in gas chromatography-mass spectrometry analysis.

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