GCMS calibration data for TCLP analysis, May 2002

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Calibration table listing response factors for deuterated standards used in TCLP analysis on May 5, 2002.

NYC-WTC_000023195–000023202

Folder label: “GCMS X 5/8/02 A 5/9/02”

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NYC 9/11 Public Portal Document Library Search Compound Report

Data File C:\HPCHEM\1\DATA\MAY0302\9577.D Vial: 50 Acq On 5 May 2002 4:02 pm Operator: Sample GC/MS SCAN 4/23 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0501.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 Cyclopentasiloxane, decamethyl Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 14.80 3.54 ug/1 288666 Naphthalene-d8 15.82 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 (80 2 Benzoic acid, 2,4-bis[(trimethylsil 370 C16H30O4Si3 010586-16-0 43 3 3,4-Dihydroxybenzyl alcohol,tris(tr 356 C16H3203Si3 068595-79-9 38 4 Benzeneacetic acid, .alpha.,4-bis[( 326 C15H26O4Si2 055334-40-2 37 Abundance Scan 1065 (14.798 min): 9577.D (-) m/ z 73.10 100.00% 73

5000 267 355

45 14.40 14.60 14.80 15.00 15.20 uI 22321— TTTTTTT m/z 267.05 108125 154 177193 323339 |i -HH4 ■ latti th ।i', |*. 35.40% m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #51266: Cyclopentasiloxane, decamethyl- 73

355 267 5000 14.40 14.60 14.80 15.00 15.20 m/z 355.10 33.73% 191207 251 .. 323339 I " 1' I'' " I' * " I'' " I' " ' I' ‘1' I p-TT-q-Ti-r-q- 11''1 ■ I' 1 ’11'' TT I'11 ’ I miz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #73975: Benzoic acid, 2,4-bis[(trimethylsilyl)oxy]-, trimet 73

14.40 14.60 14.80 15.00 15.20 5000 355 m/z 356.10 12.08% 45

133149 193 223 281 "11f TTTTRLPT WTIPTTTTTWTPTTITTTTTTTT i" " i m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #49868:3,4-Dihydroxybenzyl alcohol,tris(trimethylsilyl)- 73 14.40 14.60 14.80 15.00 15.20 m/z 268.05 9.15% 267 5000 179 356 45 147 " ' i " " I " " r ■ " i " '' i ‘ I ' i " " i" 209 237 , 11001—001—————22—11 " i ‘312‘ i " " i" i' " ‘ i _1 m/z—> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 14.40 14.60 14.80 15.00 15.20

9577.D GCMS0501.M Tue May 07 15:01:47 2002 Page 2

NYC-WTC_000023201

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