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GCMS surrogate recovery data for sample AE04945, April 2002

Machine-extracted title · confidence 100%

Record of surrogate compound recovery rates for sample AE07634 analyzed on April 30, 2002.

NYC-WTC_000040212–000040229

Folder label: “GCMS X 4/3/02 A 4/10/02

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Scanned page image, NYC-WTC_000040228
OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\MAR3002\4945.D Vial: 12 Acq On : 30 Mar 2002 1:52 am Operator: Sample : gc/ms scan 3/6 Inst : GC/MS 2 09 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 Cyclopentasiloxane, decamethyl Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

14.84 0.84 ug/1 133465 Naphthalene-d8 15.88

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 53 2 3,4-Dihydroxybenzyl alcohol, tris(tr 356 C16H3203Si3 068595-79-9 50 3 Benzoic aci 2-[(trimethylsilyl)ox 282 C13H2203Si2 003789-85-3 38 4 Benzeneethanamine, N- [ (pentafluorop 475 C21H26F5NO2Si2 055429-85-1 38 Abundance Scan 1067 (14.843 min): 4945.D (-) m/z73.dpibo.00% 73

5000- 267 355 -------................ 45 108 133 154 177 193 223 251 i 14.60 14.80 15.00 15.20 II 323 339 ] ■ i11 " ।1'111'1111 TITTT TIIPTTT m/z 267.00 39.77% miz-? 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #51266: Cyclopentasiloxane, decamethyl- 73

355 267 / 5000 I ' ' 14.60 14.80 15.00 15.20 m/z 355.05 37.33% 191 207 251 323 339 I 11"11‘111-‘!——-—TTT110‘"1"—u-—TTTTTVTITTTE TITTT ' ■ 11'' । 'l >' 11 f < ■ m/z-> 40 60. 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance a / i at - . 73 —.... - 14.60 14.80 15.00 15.20 267 5000 179 m/z 356.05 14.74% 356 45 147 209 237 312 341 ‘1‘1‘11"1171111111E-11—EI"TTTE11111IIII1OOIUIIIDIIOISIIUTTI—VpTT miz-P 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #72300: Benzoic acid, 2-!(trimethylsilyi)oxyj-, trimethyisi > ■ i ■ ■ ' ■ i 1 ' 1 r'i 1 । । । । ■ । 73 14.60 14.80 15.00 15.20 m/ Z 2 68.00 11.40% 267 5000

45

m/z-> ‘II 40 92 135151 175 193 209 233249 ( 11 ‘'1' । " '' i'''' i''' ‘ i'1' ‘ i'''' i''1' i1''11''1' i'11' i ‘11 11'''' i''1 1111111 1111111 -4........ 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 14.60 14.80 15.00 15.20

4945.D GCMS0308.M Tue Apr 02 11:08:13 2002 Page 1

NYC-WTC_000040228

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NYC-WTC_000040228Source: NYC Law Department, mirrored locally

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