NYC 9/11 Public Portal Document
Library Search Compound Report
Data File : C:\HPCHEM\l\DATA\MAR3002\4945.D Vial: 12
Acq On : 30 Mar 2002 1:52 am Operator:
Sample : gc/ms scan 3/6 Inst : GC/MS 2 09
Mise Multiplr: 1.00
MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator)
Title : 209 625/TCLP calibration table
Library : C:\DATABASE\NBS75K.L
*********************************************************************
Peak Number 1 Cyclopentasiloxane, decamethyl Concentration Rank 1
R.T. EstConc Area Relative to ISTD R.T.
14.84 0.84 ug/1 133465 Naphthalene-d8 15.88
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 53
2 3,4-Dihydroxybenzyl alcohol, tris(tr 356 C16H3203Si3 068595-79-9 50
3 Benzoic aci 2-[(trimethylsilyl)ox 282 C13H2203Si2 003789-85-3 38
4 Benzeneethanamine, N- [ (pentafluorop 475 C21H26F5NO2Si2 055429-85-1 38
Abundance Scan 1067 (14.843 min): 4945.D (-) m/z73.dpibo.00%
73
5000- 267 355
-------................
45 108 133 154 177 193 223 251 i 14.60 14.80 15.00 15.20
II 323 339
]
■ i11 " ।1'111'1111 TITTT TIIPTTT m/z 267.00 39.77%
miz-? 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360
Abundance #51266: Cyclopentasiloxane, decamethyl-
73
355
267 /
5000 I ' '
14.60 14.80 15.00 15.20
m/z 355.05 37.33%
191 207 251 323 339 I
11"11‘111-‘!——-—TTT110‘"1"—u-—TTTTTVTITTTE TITTT ' ■ 11'' । 'l >' 11 f < ■
m/z-> 40 60. 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360
Abundance a / i at - .
73
—.... -
14.60 14.80 15.00 15.20
267
5000 179 m/z 356.05 14.74%
356
45 147
209 237 312 341
‘1‘1‘11"1171111111E-11—EI"TTTE11111IIII1OOIUIIIDIIOISIIUTTI—VpTT
miz-P 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360
Abundance #72300: Benzoic acid, 2-!(trimethylsilyi)oxyj-, trimethyisi > ■ i ■ ■ ' ■ i 1 ' 1 r'i 1 । । । । ■ ।
73 14.60 14.80 15.00 15.20
m/ Z 2 68.00 11.40%
267
5000
45
m/z->
‘II
40
92 135151 175 193 209 233249 (
11 ‘'1' । " '' i'''' i''' ‘ i'1' ‘ i'''' i''1' i1''11''1' i'11' i ‘11 11'''' i''1 1111111 1111111 -4........
60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 14.60 14.80 15.00 15.20
4945.D GCMS0308.M Tue Apr 02 11:08:13 2002 Page 1
NYC-WTC_000040228
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