GCMS analysis report for sample AE01154, March 2002

Machine-extracted title · confidence 95%

Analytical results page for sample AE01154 processed on March 4, 2002, showing surrogate recovery data.

NYC-WTC_000009676–000009685

Folder label: “GCMS X 1/14/02 A 3/4/02”

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\FEB21O2\1154.D Vial: 68 Acq On : 24 Feb 2002 11:00 am Operator: Sample : gc/ms scan 2/21 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 Cyclopentasiloxane, decamethyl Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

14.92 0.75 ug/1 53190 Naphthalene-d8 15.97

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 53 2 Benzoic acid, 2,5-bis(trimethylsilo 370 C16H30O4Si3 003618-20-0 35 3 Benzoic acid, 2,6-bis[(trimethylsil 370 C16H30O4Si3 003782-85-2 32 4 Benzoic acid, 2-[(trimethylsilyl)ox 282 C13H2203Si2 003789-85-3 28 Abundance Scan 1076 (14.922 min): 1154.D(-) m/z 73.00 100.00%] 73

5000 267 355

45 ■ k 133 154 , 193 223 251 1___ 14.60 14.80 15.00 15.20 ' ' ‘ 323339 1 T1’7 ‘1‘-"11378101110—mm001—003"1120100/1 ■ i ■ ■1' i “ ‘ * i1 ‘ ’ i ■ •" I m/z 266.90 39.97% miz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #51266: Cyclopentasiloxane, decamethyl- 73

355 267 5000 14.60 14.80 15.00 15.20 ' ' ' m/z 355.0 30.16% 191207 251 k 323339 | ‘1′01′10′11111151019191—00001 • ■ i “ ■ ■ i ■ “ • i “ ‘ ■ i " ■ ‘ i mz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 'Abundance 78. B-nzgk 73 355 14.60 14.80 15.00 15.20 5000 m/z 356.05 12.46 45 147 179 207223 267282297 370 ‘ I" ■ ■ i ■ ■111 ■ i ■ ■ ■ ■ i " " i ‘111111" 11" 11111' I " 1'' 1 Ir 1'11' • ■ ■ i ■1 “ i ■ • ■ ■ i ‘ ‘i"“ i m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #51296: Benzoic acid, 2,6-bis[(trimethylsilyl)oxy]-, trimet ‘ ‘ i ‘ ‘ ‘ ' i ‘ ' 1 i ‘ ‘ ‘ i 1 ' ‘ ' i 73 355 14.60 14.80 15.00 15.20 m/z 74.00 10.72% 5000

147 267

m/z-> 47 I ‘‘ i" ..0000777. 208,.2/9282 370 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 ‘ 14.60 14.80 15.00 15.20

1154.D GCMS0208.M Fri Mar 01 09:08:06 2002 Page 2

NYC-WTC_000009684

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