GCMS blank analysis report, May 6, 2002

NYC 9/11 Public Portal Document Library Search Compound Report

Data File C: \HPCHEM\1\DATA\MAY0302\LB.D Vial: 3 Acq On 3 May 2002 3:58 pm Operator: Sample GC/MS SCAN 4/24 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0501.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 Cyclopentasiloxane, decamethyl Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

14.80 2.28 ug/1 194181 Naphthalene-d8 15.83

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 2 Benzeneeth amine, N-[(pentafluorop 563 C24H34F5NO3Si3 055429-13-5 3 3,4-Dihydn oxybenzyl alcohol,tris(tr 356 C16H3203Si3 068595-79-9 43 4 Phenethylammine, N-methyl-.beta.,3,4 399 C18H37NO3Si3 010538-85-9 40 Abundance 1 Scan 1065 (14.800 min): LB.D (-) m/ z 73.10 100.00% 73

5000 267 355 I I I < I 1 I I Ti TI I Cp I I I I I I I

45 14.40 14.60 14.80 15.00 15.20 L I J 99 125 154 193 223 . i ’i ’ 1 । i r i । 11 I * r । I । i 1 । T 323 m/z 267.05 34.75% m/z->____ 50 _ 100 150 200 250 300 350 400 450 500 550 Abundance #51266: Cyclopentasiloxane, decamethyl- 73

355 267 5000 । । t । । । i । । I [ I । । i ] i i i । । । r 14.40 14.60 14.80 15.00 15.20 m/ Z 355.10 34.03% 207 323, j 1 1 i ' m/z—> 50 100 150 250 300 350 400 200 450 500 550 Abundance #74706: Benzeneethanamine, N-[(pentafluoraphenyl)methylene] 73 355 1t/"/‘11T/"/TI/""CIT/UIIIET 14.40 14.60 14.80 15.00 15.20 5000 m/ z 356.10 12.88%

45 208 251 281 , 386 458 548 i । | i i i I | i i I i i I T 11 I I I 1l I I I I I I T 1 r I 171 I l 1 I I 1 1 i 1 1 1 1 i 1 ’ 1 1 1 1 1 m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #49868: 3,4-Dihydroxybenzyl alcohol,tris(trimethylsilyl)- 73 14.40 14.60 14.80 15.00 15.20 m/z 267.95 8.89% 267 5000 179 356 45 147 ...... .. 209 237, ‘ 1 1 ' 1 I-“I | i I I i q I T ———— । i i ।312। । i / ] n । i । । r i j- i । i i i T i । । । । i r [ I I I I I 11 I f [ 1 I I I [ I I I I I I i

m/z-> 50 100 150 200 250 300 350 400 450 500 550 14.40 14.60 14.80 15.00 15.20

LB.D GCMS0501.M Mon May 06 10:51:25 2002 Page 2

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