GCMS analysis results for sample AE07313, April 2002

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Library Search Compound Report

Data File C : \HPCHEM\ 1 \DATA\ APRO3027313.D Vial: 9 Acq On 3 Apr 2002 8:35 pm Operator: Sample gc/ms scan 3/28 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0403.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 Cyclopentasiloxane, decamethyl Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

14.84 1.26 ug/1 190513 Naphthalene-d8 15.88 Hit# Of 5 Tentative ID MW MolForm CAS# Qual 1 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 64 2 Benzoic acid, /2,4-bis[(trimethylsil 370 C16H30O4Si3 010586-16-0 47 3 Phenethylamine, N-methyl-.beta.,3,4 399 C18H37NO3Si3 010538-85-9 38 4 N- (Trifluoroacetyl) -N,O,O',0' 1-tetr 553 C22H42F3NO4Si4 000000-00-0 32 Abundance Scan 1067 (14.843 min): 7313.D (-) m/z 73.00 100.00% 73

5000- 267 355 , | [ ' I i i | i — i | i I i i । i r

45 14.60 14.80 15.00 15.20 , 108 133 154 177193 223 251 । 323339 I . 1 I''111 ] । i । i । । । j rr । । । r । । । । । । ।T । । । । i । m/ z 2 67.00 42.89% rn/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #51266: Cyclopentasiloxane, decamethyl- 73

355 5000 267 TTI J I 1 ' 14.60 14.80 15.00 15.20 m/z 355.05 42.14% 191207 251 323339 | I ‘ 1 "I 1 1 1 1 I'' 111 1 1 ' H1 1 1 ' I r 1'11' ■ ■' i I' " ' I I M 1 1 I 171 mfe-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #73975: Benzoic acid, 2,4-bis[(trimethylsilyl)oxy]-, trimet 73 .............. ).................. 1 1 I 1 1 1 1 I ' 1 I I I ‘ I < I I ’ I 14.60 14.80 15.00 15.20 5000 355 m/z 356.05 14.95% 45

133149 193 I 370 223 281 1 1 | 1 / 1 > । i i i i । i i i i j i ri i । i i i i । i 7 i । । । । j i । । । r । । r i' r i | I i i । । 'i i i i । 11 f i p i i i [ i i i" i । rr 1' i " '11 " " i m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #74239: Phenethylamine, N-methyl-.beta.,3,4-tris(trimethyls ..... ... 73 14.60 14.80 15.00 15.20 m/z 267.90 10.89% 5000 355

miz- LU40 60 i 88 ........ 130147 193 267 | । 1 > । ] । । । 1 | i । । I | I I I I ^“1 "I I r I i i t71 I | rrrrrur r 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 294 I 1 ‘ L 14.60 14.80 15.00 15.20

7313.D GCMS0403.M Tue Apr 09 13:08:08 2002 Page 3

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