Laboratory report of GCMS analysis for sample AE09680 conducted on May 23, 2002, showing surrogate recovery data.
NYC-WTC_000023828–000023834Folder label: “GCMS X 5/9/02 A 5/20/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document Library Search Compound Report
Data File C: \HPCHEM\ 1 \DATA\MAY06 02\9680.D Vial: 23 Acq On 7 May 2002 1:51 pm Operator: Sample GC/MS SCAN 4/25 FB Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS0501.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L
Peak Number 1 2-Pentanone, 4-hydroxy-4-methy Concentration Rank 1
R.T. EstConc Area Relative to ISTD R.T.
8.16 11.17 ug/1 855555 1,4-Dichlorobenzene-d4 12.19
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 2-Pentanone, 4-hydroxy-4-methyl- 116 C6H1202 000123-42-2 78 2 CH2=CHCH2C(O)OCH3 100 C5H802 003724-55-8 9 3 Acetope 58 C3H60 000067-64-1 7 4 5-Hexen-2-one 98 C6H10O 000109-49-9 5 Abundance Scan 341 (8.162 min): 9680.D (-) m/z 43.05 100.00%| 43
5000 59
101 7.80 8.00 8.20 8.40 8.60 m/z-> .................................... 38, ' i ‘ 10 53., ■ I 1 1 1 1 1 1 1 ' ' f 1 +THTT 20 30 40 50 60 70 80 69 83 ' i ' ' ' ' i '1 ■ i ' 90 4 m/ z 100 110 59.10 42.06%| Abundance #64274:2-Pentanone, 4-hydroxy-4-methyl- 43
_________ __ P ... 5000 59 7 80 8.00 8.20 8.40 8.60 m/z 58.10 16.33% 27 101
m/z-> i ■ ■ ■ ■ । 1 10 20 - 30 40 50 +49+ I60,11481111,83 70 80 — .......... 90 1....... 100 110 Abundance #1448: CH2=CHCH2C(O)OCH3 43 ..... . 7 80 8.00 8.20 8.40 8.60 5000 m/z 101.15 13.18%
........................ 381 1 i 1 ' ' ' i ' ■ ■ ■ i ■ ■ ' 1 I1 * T 72 100 mlz-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #94: Acetone .......... / 43 7.80 8.00 8.20 8.40 8.60 m/z 41.05 6.85% 5000 15 58 27
m/z—> ---+ 10 20 30 40 1 i 1 1 50 ' i ' ' ' ' i ' ' ' ' i ' 1 1 ' i ■ ' 1 ' 1 1 1 1 1 1 1 -- m , 1. j T r -. r 60 70 80 90 100 110 7.80 8.00 8.20 8.40 8.60
9680.D GCMS0501.M Thu May 09 11:25:49 2002 Page 1
NYC-WTC_000023833
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NYC-WTC_000023701
Laboratory report of GCMS analysis for sample AE10063 conducted on May 23, 2002, showing surrogate recovery data.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000023738
Laboratory report of GCMS analysis for sample AE10065 conducted on May 23, 2002, showing surrogate recovery data.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000023684
Laboratory report of GCMS analysis for sample AE10062 conducted on May 23, 2002, showing surrogate recovery data.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000023754
Laboratory report of GCMS analysis for sample AE09654 conducted on May 23, 2002, showing surrogate recovery data.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000022902
Reviewed data file listing retention times and response factors for deuterated internal standards.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000023055
GCMS calibration table and instrument data for TCLP analysis recorded on May 5-7, 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000013217
Calibration table listing response factors for deuterated standards and target compounds used in gas chromatography-mass spectrometry analysis.
1 shared topics · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000013251
Calibration table listing response factors for deuterated standards and target compounds used in gas chromatography-mass spectrometry analysis.
1 shared topics · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000013184
Calibration table listing response factors for deuterated standards and target compounds used in gas chromatography-mass spectrometry analysis.
1 shared topics · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000013277
Calibration table listing response factors for deuterated standards and target compounds used in gas chromatography-mass spectrometry analysis.
1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000045490
Technical document displaying GCMS calibration data and compound retention times for sample AE09448 processed in early May 2002.
1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000013146
Calibration table listing response factors for deuterated standards and target compounds used in gas chromatography-mass spectrometry analysis.
1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000023646
Department of Environmental Protection administrative record sheet for World Trade Center site activities dated May 2002.
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NYC-WTC_000023647
Technical data file header page from a GCMS analysis run associated with the World Trade Center site in May 2002.
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NYC-WTC_000023649
Laboratory report showing GC/MS blank analysis for sample AE09676 with non-detect results for volatile organic compounds.
Filed in the same folder
NYC-WTC_000023662
Laboratory report showing GC/MS calibration data for volatile organic compounds analyzed on May 20-21, 2002.
Filed in the same folder
NYC-WTC_000023666
Laboratory report showing GC/MS reference analysis for sample AE09676 with quantitative results for volatile organic compounds.
Filed in the same folder