GCMS analysis results for sample AE10520, May 2002

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Data File : C:\HPCHEM\l\DATA\MAY1002\10520.D Vial: 43 Acq On : 12 May 2002 7:02 am Operator: Sample : gc/ms scan 5/2 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0510.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L Peak Number 1 2-Pentanone, 4-hydroxy-4-methy Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 8.14 12.23 ug/1 1090640 1,4-Dichlorobenzene-d4 12.16 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Pentanone, 4-hydroxy-4-methyl- 116 C6H1202 000123-42-2 64 2 CH2=CHCH2C (O) OCH3 100 C5H802 003724-55-8 9 3 Acetone 58 C3H60 000067-64-1 7 4 5-Hexen-2-one 98 C6H10O 000109-49-9 7 Abundance Scan 338 (8.136 min): 10520.D (-) m/z 43.05 100.00% 43

5000 59

101 1 1 T 1 ' 11 1 1 1 1 1 1 1 UBl 1 1 1 1 ' I ' 53 , | 7.80 8.00 8.20 8.40 ............ .1* —I r i 1111111’1’ 69 - i ■ ■ ■ . 83 ■ ■ । . । ■ ■. I J. । । . । . m/z 59.10 43.84% m/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #64274:2-Pentanone, 4-hydroxy-4-methyl- 43

5000 FTT‘‘‘‘Tu‘I‘ CnT, . । । . 59 7.80 8.00 8.20 8.40 m/z 58.10 16.30% 27 101

mlz—> ..... 10 20 I,30... 40 +9 50 <T . > ' . I ' 60 70. 83 1 i 1'1 1 ' i 80 90 । J' 1 1 । । ' 100 110 Abundance #1448: CH2=CHCH2C(O)OCH3 43 ................. I I I I I I I P I I I I I I I ................ I I I I t t I I I

7.80 8.00 8.20 8.40 5000 m/z 101.15 14.24%

....... 38 i ' ' ' 1 i ■ ■ 1 ' i 1 ' 1 1 I 1 TIIPI 56 72 100 m/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #94: Acetone I I | ’ I n I | i i r ! ] iiil k I t ! | ) 43 7.80 8.00 8.20 8.40 m/z 41.05 7.18% 5000 15 58 27 ,1 ,1 ,1 111 .|.......... il............. m/z—> 10 1 1 1 > 1 * I I 1 ' > I I 20 30 40 ‘5o‘ 60 । 1 1 1 1 । 1 ■ ■ 1 । 1 1 1 ■ । 1 ' ' ' । 1 1 1 1 । 1 70 80 90 100 110 7.80 8.00 8.20 8.40

10520.D GCMS0510.M Thu May 16 15:45:02 2002 Page 1

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