GCMS results for sample AE10065, May 2002

NYC 9/11 Public Portal Document

Library Search Compound Report Data File C:\HPCHEM\1\DATA\MAY0302\10065.D Vial: 38 Acq On 5 May 2002 4:16 am Operator: Sample GC/MS SCAN 4/26 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0501.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L Peak Number 1 2-Pentanone, 4-hydroxy-4-methy Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 8.15 13.17 ug/1 945970 1,4-Dichlorobenzene-d4 12.20 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Pentanone, 4-hydroxy-4-methyl- 116 C6H1202 000123-42-2 78 2 3 -Hydroxy- 2 - pentanone 102 C5H10O2 003142-66-3 9 3 CH2=CHCH2C(O)OCH3 100 C5H802 003724-55-8 9 4 Acetone 58 C3H60 000067-64-1 7 Abundance Scan 340 (8.155 min): 10065.D (-) m/z 43.05 100.00% 43

5000 59

101 7.80 8.00 8.20 8.40 8.60 ......... 38 / ' 1 i 1 ' ' ' i ‘ ‘ ‘ ' i 1 ' ‘ 1 [ ■ 53 , ' I ' 1,1,1 I 69 83 | m/z 59.05 42.89% m/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #64274: 2-Pentanone, 4-hydroxy-4-methyl- 43

5000 59 7.80 8.00 8.20 8.40 8.60 m/z 58.10 15.93% 27 101

miz—> 10 20 1,/ 30 ..40 +49 50 60 I ■ ■ ■ ■ i ■ .' ■ 70 83 - ■ i ''■ 80 90 100 110 Abundance #1691:3-Hydroxy-2-pentanone 31 59

7.80 8.00 8.20 8.40 8.60 5000 m/z 101.15 13.28% 45 15 , 66 73 84 102 ' ‘ i ' ■ ' ' i ■ ' ■ ■ i ' ■ ■ 1 i ■ 1 1 i ' ' m/z—> 10 20 30 40 50 60 70 80 90 100 110 Abundance #1448: CH2=CHCH2C(O)OCH3 43 7.80 8.00 8.20 8.40 8.60 m/ z 41.05 7.05%| 5000

m/z—> ....... 20 38 l1 1 1 1 I • • • • i 1 1 ' 1 i 1 10 30 40 .750 60 70 .......... . 80 90 100 । । । | । । i । । । 100 110 TP —77 r ! TT-Tr 7.80 8.00 8.20 8.40 8.60

10065.D GCMS0501.M Tue May 07 12:01:00 2002 Page 1

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