GCMS results for sample AE10063, May 2002

NYC 9/11 Public Portal Document Library Search Compound Report Data File C:\HPCHEM\1\DATA\MAY0302\10063.D Vial: 36 Acq On 5 May 2002 2:19 am Operator: Sample GC/MS SCAN 4/26 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0501.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L Peak Number 1 2-Pentanone, 4-hydroxy-4-methy Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 8.16 15.77 ug/1 1133000 1,4-Dichlorobenzene-d4 12.19 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 2-Pentanone, 4 - hydroxy- 4 -methyl - 116 C6H1202 000123-42-2 64 2 3-Hydroxy-2-pentanone 102 C5H10O2 003142-66-3 9 3 CH2=CHCH2C(O)OCH3 100 C5H802 003724-55-8 9 4 N,N‘ Bis(2-methyl-2-nitrosopentan-4 258 C12H22N2O4 094514-30-4 9 Abundance । Scan 341 (8.162 min): 10063.D (-) m/ z 43.05 100.00% 43

5000 59

101 7 80 8.00 8.20 8.40 8.60

m/z-> .................................... 38, i ■ 1 1 10 ■ i ■ 20 ■ ■ 1 i ■ ' 30 ■ 1 r' 40 ---H 50 53 , 60 69 70 80 83 90 4 m/z 100 110 59.10 43.11% Abundance #64274: 2-Pentanone, 4-hydroxy-4-methyl- 43

5000 59 7.80 8.00 8.20 8.40 8.60 m/z 58.10 16.45% 27 I I I +49+ 83 101 mfe-> 10 20 30 40 50 60 70 - 80 90 100 110 Abundance #1691:3-Hydroxy-2-pentanone 31 59 7.80 8.00 8.20 8.40 8.60 5000 m/z 101.15 13.69% 45 15 .... |..... II...... ' ' I 1 ' ‘ ‘ ' 1 ' 1 I ' ' 1 ' I 1 i ■ ■ , 66 73 84 102 । | ■ ■ ■ ■ । > ■ ■ ■ । - ■ ■ ■ । . ■ ■ ■ । ‘ । . rnfz-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #1448: CH2=CHCH2C(O)OCH3 40 7 80 8.00 8.20 8.40 8.60 m/z 41.00 7.03% 5000

58 72 100 —..... 38,1 II// m/z—> 10 20 30. 40 50 60 70 80 90 100 110 7.80 8.00 8.20 8.40 8.60

10063.D GCMS0501.M Tue May 07 12:00:28 2002 Page 1

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